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|a 10.1002/mrc.5202
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|a eng
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|a Lankhorst, Peter P
|e verfasserin
|4 aut
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|a Discrimination of stereoisomers by one-dimensional 13 C NMR
|b All 16 stereoisomers of 4-hydroxy-α-tocopherol resolved
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|c 2021
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|a Text
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|a ƒaComputermedien
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|a ƒa Online-Ressource
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|a Date Completed 25.10.2021
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|a Date Revised 25.10.2021
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a © 2021 DSM Food Specialties B.V. Magnetic Resonance in Chemistry published by John Wiley & Sons Ltd.
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|a All 16 resolved! A vitamin E-derived compound containing four chiral centers is the first example where all stereoisomers, that is, eight diastereomeric pairs of enantiomers, could be discriminated in a single NMR run. Measurement at 176 MHz in the presence of Pirkle's alcohol as a chiral solvating agent is a relatively robust, simple, easy-to-set-up, and fast method
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|a Letter
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|a Duchateau, Alexander L L
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|a Netscher, Thomas
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|t Magnetic resonance in chemistry : MRC
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|g 59(2021), 11 vom: 11. Nov., Seite 1146-1153
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