In situ semi-quantitative analysis of zinc dissolution within nanoporous silicon by X-ray absorption fine-structure spectroscopy employing an X-ray compatible cell

The in situ study of the discharge process in a zinc-based half-cell employing a porous electrode as a structural scaffold is reported. The in situ characterization has been performed by synchrotron X-ray absorption fine-structure spectroscopy and, for this purpose, an inexpensive, simple and versat...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 26(2019), Pt 1 vom: 01. Jan., Seite 119-123
1. Verfasser: Muñoz-Noval, Álvaro (VerfasserIn)
Weitere Verfasser: Fukami, Kazuhiro, Koyama, Akira, Kuruma, Takuya, Hayakawa, Shinjiro
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2019
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article in situ XAFS cell porous electrodes zinc negative electrodes
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520 |a The in situ study of the discharge process in a zinc-based half-cell employing a porous electrode as a structural scaffold is reported. The in situ characterization has been performed by synchrotron X-ray absorption fine-structure spectroscopy and, for this purpose, an inexpensive, simple and versatile electrochemical cell compatible with X-ray experiments has been designed and described. The experimental results reported here have been employed to semi-quantify the dissolved and undissolved zinc species during the discharge, allowing the cell feasibility to be tested and to better understand the functioning of the zinc half-cell based on porous electrodes 
650 4 |a Journal Article 
650 4 |a in situ XAFS cell 
650 4 |a porous electrodes 
650 4 |a zinc negative electrodes 
700 1 |a Fukami, Kazuhiro  |e verfasserin  |4 aut 
700 1 |a Koyama, Akira  |e verfasserin  |4 aut 
700 1 |a Kuruma, Takuya  |e verfasserin  |4 aut 
700 1 |a Hayakawa, Shinjiro  |e verfasserin  |4 aut 
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