In situ semi-quantitative analysis of zinc dissolution within nanoporous silicon by X-ray absorption fine-structure spectroscopy employing an X-ray compatible cell
The in situ study of the discharge process in a zinc-based half-cell employing a porous electrode as a structural scaffold is reported. The in situ characterization has been performed by synchrotron X-ray absorption fine-structure spectroscopy and, for this purpose, an inexpensive, simple and versat...
| Veröffentlicht in: | Journal of synchrotron radiation. - 1994. - 26(2019), Pt 1 vom: 01. Jan., Seite 119-123 |
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| Format: | Online-Aufsatz |
| Sprache: | English |
| Veröffentlicht: |
2019
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| Zugriff auf das übergeordnete Werk: | Journal of synchrotron radiation |
| Schlagworte: | Journal Article in situ XAFS cell porous electrodes zinc negative electrodes |
| Zusammenfassung: | The in situ study of the discharge process in a zinc-based half-cell employing a porous electrode as a structural scaffold is reported. The in situ characterization has been performed by synchrotron X-ray absorption fine-structure spectroscopy and, for this purpose, an inexpensive, simple and versatile electrochemical cell compatible with X-ray experiments has been designed and described. The experimental results reported here have been employed to semi-quantify the dissolved and undissolved zinc species during the discharge, allowing the cell feasibility to be tested and to better understand the functioning of the zinc half-cell based on porous electrodes |
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| Beschreibung: | Date Completed 30.01.2019 Date Revised 30.01.2019 published: Print-Electronic Citation Status PubMed-not-MEDLINE |
| ISSN: | 1600-5775 |
| DOI: | 10.1107/S1600577518014789 |