|
|
|
|
| LEADER |
01000naa a22002652 4500 |
| 001 |
NLM286219409 |
| 003 |
DE-627 |
| 005 |
20231225051204.0 |
| 007 |
cr uuu---uuuuu |
| 008 |
231225s2018 xx |||||o 00| ||eng c |
| 024 |
7 |
|
|a 10.1107/S1600577518005945
|2 doi
|
| 028 |
5 |
2 |
|a pubmed24n0954.xml
|
| 035 |
|
|
|a (DE-627)NLM286219409
|
| 035 |
|
|
|a (NLM)29979164
|
| 040 |
|
|
|a DE-627
|b ger
|c DE-627
|e rakwb
|
| 041 |
|
|
|a eng
|
| 100 |
1 |
|
|a Gog, Thomas
|e verfasserin
|4 aut
|
| 245 |
1 |
0 |
|a Performance of quartz- and sapphire-based double-crystal high-resolution (∼10 meV) RIXS monochromators under varying power loads
|
| 264 |
|
1 |
|c 2018
|
| 336 |
|
|
|a Text
|b txt
|2 rdacontent
|
| 337 |
|
|
|a ƒaComputermedien
|b c
|2 rdamedia
|
| 338 |
|
|
|a ƒa Online-Ressource
|b cr
|2 rdacarrier
|
| 500 |
|
|
|a Date Revised 20.11.2019
|
| 500 |
|
|
|a published: Print-Electronic
|
| 500 |
|
|
|a Citation Status PubMed-not-MEDLINE
|
| 520 |
|
|
|a In the context of a novel, high-resolution resonant inelastic X-ray scattering spectrometer, a flat-crystal-based quartz analyzer system has recently been demonstrated to provide an unprecedented intrinsic-energy resolution of 3.9 meV at the Ir L3 absorption edge (11.215 keV) [Kim et al. (2018) Sci. Rep. 8, 1958]. However, the overall instrument resolution was limited to 9.7 meV because of an 8.9 meV incident band pass, generated by the available high-resolution four-bounce Si(844) monochromator. In order to better match the potent resolving power of the novel analyzer with the energy band pass of the incident beam, a quartz(309)-based double-bounce, high-resolution monochromator was designed and implemented, expected to yield an overall instrument resolution of 6.0 meV. The choice of lower-symmetry quartz is very attractive because of its wealth of suitable near-backscattering reflections. However, it was found that during room-temperature operation typical levels of incident power, barely affecting the Si monochromator, caused substantial thermal distortions in the first crystal of the quartz monochromator, rendering it practically unusable. Finite-element analyses and heat-flow analyses corroborate this finding. As a high-flux, lower resolution (15.8 meV) alternative, a two-bounce sapphire(078) version was also tested and found to be less affected than quartz, but notably more than silicon
|
| 650 |
|
4 |
|a Journal Article
|
| 650 |
|
4 |
|a RIXS
|
| 650 |
|
4 |
|a X-ray optics
|
| 650 |
|
4 |
|a high-resolution monochromators
|
| 650 |
|
4 |
|a non-traditional crystal materials
|
| 650 |
|
4 |
|a resonant inelastic X-ray scattering
|
| 700 |
1 |
|
|a Casa, Diego M
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Knopp, Jonathan
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Kim, Jungho
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Upton, Mary H
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Krakora, Richard
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Jaski, Alan
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Said, Ayman
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Yavaş, Hasan
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Gretarsson, Hlynur
|e verfasserin
|4 aut
|
| 700 |
1 |
|
|a Huang, Xian Rong
|e verfasserin
|4 aut
|
| 773 |
0 |
8 |
|i Enthalten in
|t Journal of synchrotron radiation
|d 1994
|g 25(2018), Pt 4 vom: 01. Juli, Seite 1030-1035
|w (DE-627)NLM09824129X
|x 1600-5775
|7 nnns
|
| 773 |
1 |
8 |
|g volume:25
|g year:2018
|g number:Pt 4
|g day:01
|g month:07
|g pages:1030-1035
|
| 856 |
4 |
0 |
|u http://dx.doi.org/10.1107/S1600577518005945
|3 Volltext
|
| 912 |
|
|
|a GBV_USEFLAG_A
|
| 912 |
|
|
|a SYSFLAG_A
|
| 912 |
|
|
|a GBV_NLM
|
| 912 |
|
|
|a GBV_ILN_40
|
| 912 |
|
|
|a GBV_ILN_350
|
| 912 |
|
|
|a GBV_ILN_2005
|
| 951 |
|
|
|a AR
|
| 952 |
|
|
|d 25
|j 2018
|e Pt 4
|b 01
|c 07
|h 1030-1035
|