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231224s2017 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.4590
|2 doi
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|a pubmed24n0897.xml
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|a eng
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1 |
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|a Haapaniemi, Esa
|e verfasserin
|4 aut
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|a Complete 1 H, 13 C{1 H}, and 31 P NMR spectral parameters of some pyrophosphates
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|c 2017
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
|b c
|2 rdamedia
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|a ƒa Online-Ressource
|b cr
|2 rdacarrier
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|a Date Completed 05.03.2018
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|a Date Revised 05.03.2018
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a Copyright © 2017 John Wiley & Sons, Ltd.
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|a The 1 H, 13 C{1 H}, and 31 P NMR spectral parameters of some pyrophosphates were determined in CDCl3 . The most complicated 1 H spectrum can be solved fully only as (A3 MN)R6 XX'R6 '(MNA3 )', where R6 (= -N(CH3 )2 ) is coupled only to phosphorus (X). Second-order coupling between phosphorus was found and solved with iterative analysis. A signal shape of one of the carbon resonance cannot be explained only with couplings. Explanation for exceptional shape was searched from molecular modeling results. Copyright © 2017 John Wiley & Sons, Ltd
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|a Journal Article
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|a 13C{1H}
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|a 1H
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|a 31P
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|a NMR
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| 650 |
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|a iterative spectral analysis
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| 650 |
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4 |
|a molecular modeling
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| 650 |
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|a pyrophosphates
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 55(2017), 9 vom: 20. Sept., Seite 804-812
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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|g volume:55
|g year:2017
|g number:9
|g day:20
|g month:09
|g pages:804-812
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|u http://dx.doi.org/10.1002/mrc.4590
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