Time- and spatial-resolved XAFS spectroscopy in a single shot : new analytical possibilities for in situ material characterization

A new concept that comprises both time- and lateral-resolved X-ray absorption fine-structure information simultaneously in a single shot is presented. This uncomplicated set-up was tested at the BAMline at BESSY-II (Berlin, Germany). The primary broadband beam was generated by a double multilayer mo...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 23(2016), Pt 3 vom: 20. Mai, Seite 769-76
1. Verfasser: Buzanich, Ana Guilherme (VerfasserIn)
Weitere Verfasser: Radtke, Martin, Reinholz, Uwe, Riesemeier, Heinrich, Emmerling, Franziska
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2016
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article divergent XAFS single-shot XAFS spatial resolution time resolution
Beschreibung
Zusammenfassung:A new concept that comprises both time- and lateral-resolved X-ray absorption fine-structure information simultaneously in a single shot is presented. This uncomplicated set-up was tested at the BAMline at BESSY-II (Berlin, Germany). The primary broadband beam was generated by a double multilayer monochromator. The transmitted beam through the sample is diffracted by a convexly bent Si (111) crystal, producing a divergent beam. This, in turn, is collected by either an energy-sensitive area detector, the so-called color X-ray camera, or by an area-sensitive detector based on a CCD camera, in θ-2θ geometry. The first tests were performed with thin metal foils and some iron oxide mixtures. A time resolution of lower than 1 s together with a spatial resolution in one dimension of at least 50 µm is achieved
Beschreibung:Date Completed 17.08.2018
Date Revised 17.08.2018
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1600-5775
DOI:10.1107/S1600577516003969