Accuracy evaluation in temperature-dependent EXAFS measurements of CdTe

The evaluation of uncertainty in temperature-dependent EXAFS measurements is discussed, considering the specific case of a recent experiment performed on CdTe. EXAFS at both Cd and Te K-edges was measured at different times and at different beamlines in a temperature range from 5 to 300 K. Attention...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 20(2013), Pt 4 vom: 07. Juli, Seite 603-13
1. Verfasser: Abd El All, N (VerfasserIn)
Weitere Verfasser: Thiodjio Sendja, B, Grisenti, R, Rocca, F, Diop, D, Mathon, O, Pascarelli, S, Fornasini, P
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2013
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article Debye model EXAFS Einstein model mean-square relative displacements thermal expansion
Beschreibung
Zusammenfassung:The evaluation of uncertainty in temperature-dependent EXAFS measurements is discussed, considering the specific case of a recent experiment performed on CdTe. EXAFS at both Cd and Te K-edges was measured at different times and at different beamlines in a temperature range from 5 to 300 K. Attention is focused on the nearest-neighbours parameters: bond thermal expansion, parallel and perpendicular mean-square relative displacements and the third cumulant. Different causes of uncertainty, a comparison of experimental results with theoretical models, the difference between EXAFS and crystallographic thermal expansions and the meaning of the third cumulant are discussed
Beschreibung:Date Completed 06.01.2014
Date Revised 14.06.2013
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1600-5775
DOI:10.1107/S0909049513012053