Shapeshifting Nanocatalyst for CO2 Conversion

© 2025 The Author(s). Advanced Materials published by Wiley‐VCH GmbH.

Détails bibliographiques
Publié dans:Advanced materials (Deerfield Beach, Fla.). - 1998. - (2025) vom: 18. Sept., Seite e09814
Auteur principal: Girotto, Gustavo Zottis (Auteur)
Autres auteurs: Jaugstetter, Maximilian, Kim, Dongwoo, Matte, Lívia P, Mishra, Tara P, Scott, Mary, Martins, Ruan M, Muniz, André R, Salmeron, Miquel, Nemsak, Slavomir, Bernardi, Fabiano
Format: Article en ligne
Langue:English
Publié: 2025
Accès à la collection:Advanced materials (Deerfield Beach, Fla.)
Sujets:Journal Article CO2 reduction reaction artificial photosynthesis in situ measurements morphology changes photocatalysis
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520 |a The conversion of CO2 into high-value chemicals through a photoreduction reaction in water is a promising route to reduce the dependence on fossil fuels. Enhancing selectivity toward hydrocarbons or alcohols can be achieved by Ag-Cu alloys. However, the stabilized surface state created by Ag-Cu interactions is still poorly understood. In this work, multi-modal in situ X-ray experiments reveals underlying mechanisms and the evolution of Ag-Cu nanoparticles under CO2 reduction reaction (CO2RR) conditions. Both morphological and chemical changes of Ag and Cu species induced by diffusion mechanics are tracked during nanocatalyst operation. The initial spheroid Ag-Cu nanoparticles are composed of a Cu-rich shell and Ag-rich core. The reduction treatment promotes Ag migration toward the surface. During photocatalytic CO2 reduction reaction, Cu atoms migrate back to the surface, forming Ag-Cu-O species. The study observes the surface oxidation of Cu(0) to Cu+ and the presence of Ag at the sub-surface region. Furthermore, nanoparticles change their shape, decreasing their specific surface area, driven by Cu diffusion during the CO2 photoreduction reaction. The results provide invaluable insights into the dynamic restructuring of the catalyst under reaction conditions and into the active species responsible for CO2 conversion 
650 4 |a Journal Article 
650 4 |a CO2 reduction reaction 
650 4 |a artificial photosynthesis 
650 4 |a in situ measurements 
650 4 |a morphology changes 
650 4 |a photocatalysis 
700 1 |a Jaugstetter, Maximilian  |e verfasserin  |4 aut 
700 1 |a Kim, Dongwoo  |e verfasserin  |4 aut 
700 1 |a Matte, Lívia P  |e verfasserin  |4 aut 
700 1 |a Mishra, Tara P  |e verfasserin  |4 aut 
700 1 |a Scott, Mary  |e verfasserin  |4 aut 
700 1 |a Martins, Ruan M  |e verfasserin  |4 aut 
700 1 |a Muniz, André R  |e verfasserin  |4 aut 
700 1 |a Salmeron, Miquel  |e verfasserin  |4 aut 
700 1 |a Nemsak, Slavomir  |e verfasserin  |4 aut 
700 1 |a Bernardi, Fabiano  |e verfasserin  |4 aut 
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773 1 8 |g year:2025  |g day:18  |g month:09  |g pages:e09814 
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