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231226s2023 xx |||||o 00| ||eng c |
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|a 10.1107/S1600577523007300
|2 doi
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|a pubmed24n1286.xml
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|a (NLM)37738031
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|a DE-627
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|e rakwb
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|a eng
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|a Greenberg, Matthew W
|e verfasserin
|4 aut
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|a In situ synchrotron X-ray total scattering measurements and analysis of colloidal CsPbX3 nanocrystals during flow synthesis
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|c 2023
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
|b c
|2 rdamedia
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|a ƒa Online-Ressource
|b cr
|2 rdacarrier
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|a Date Revised 10.02.2024
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a open access.
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|a In situ X-ray scattering measurements of CsPbX3 (X = Cl, Br, I) nanocrystal formation and halide exchange at NSLS-II beamlines were performed in an automated flow reactor. Total scattering measurements were performed at the 28-ID-2 (XPD) beamline and small-angle X-ray scattering at the 16-ID (LiX) beamline. Nanocrystal structural parameters of interest, including size, size distribution and atomic structure, were extracted from modeling the total scattering data. The results highlight the potential of these beamlines and the measurement protocols described in this study for studying dynamic processes of colloidal nanocrystal synthesis in solution with timescales on the order of seconds
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|a Journal Article
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|a X-ray total scattering
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|a nanocrystals
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|a nucleation
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|a pair distribution function
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|a perovskites
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|a small-angle X-ray scattering
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|a Lin, Cheng Hung
|e verfasserin
|4 aut
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|a Chodankar, Shirish
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Ghose, Sanjit K
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Journal of synchrotron radiation
|d 1994
|g 30(2023), Pt 6 vom: 01. Nov., Seite 1092-1099
|w (DE-627)NLM09824129X
|x 1600-5775
|7 nnns
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| 773 |
1 |
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|g volume:30
|g year:2023
|g number:Pt 6
|g day:01
|g month:11
|g pages:1092-1099
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|u http://dx.doi.org/10.1107/S1600577523007300
|3 Volltext
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|d 30
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|e Pt 6
|b 01
|c 11
|h 1092-1099
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