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231226s2023 xx |||||o 00| ||eng c |
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|a 10.1021/acs.chemmater.2c02639
|2 doi
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|a pubmed24n1179.xml
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|a (DE-627)NLM353795011
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|a (NLM)36873624
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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|a Ying, Bixian
|e verfasserin
|4 aut
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|a Monitoring the Formation of Nickel-Poor and Nickel-Rich Oxide Cathode Materials for Lithium-Ion Batteries with Synchrotron Radiation
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|c 2023
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
|b c
|2 rdamedia
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|a ƒa Online-Ressource
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|2 rdacarrier
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|a Date Revised 07.03.2023
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|a published: Electronic-eCollection
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|a Citation Status PubMed-not-MEDLINE
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|a © 2023 The Authors. Published by American Chemical Society.
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|a The syntheses of Ni-poor (NCM111, LiNi1/3Co1/3Mn1/3O2) and Ni-rich (NCM811 LiNi0.8Co0.1Mn0.1O2) lithium transition-metal oxides (space group R3̅m) from hydroxide precursors (Ni1/3Co1/3Mn1/3(OH)2, Ni0.8Co0.1Mn0.1(OH)2) are investigated using in situ synchrotron powder diffraction and near-edge X-ray absorption fine structure spectroscopy. The development of the layered structure of these two cathode materials proceeds via two utterly different reaction mechanisms. While the synthesis of NCM811 involves a rock salt-type intermediate phase, NCM111 reveals a layered structure throughout the entire synthesis. Moreover, the necessity and the impact of a preannealing step and a high-temperature holding step are discussed
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|a Journal Article
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|a Fitzpatrick, Jack R
|e verfasserin
|4 aut
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|a Teng, Zhenjie
|e verfasserin
|4 aut
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|a Chen, Tianxiang
|e verfasserin
|4 aut
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|a Lo, Tsz Woon Benedict
|e verfasserin
|4 aut
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|a Siozios, Vassilios
|e verfasserin
|4 aut
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|a Murray, Claire A
|e verfasserin
|4 aut
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|a Brand, Helen E A
|e verfasserin
|4 aut
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|a Day, Sarah
|e verfasserin
|4 aut
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|a Tang, Chiu C
|e verfasserin
|4 aut
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|a Weatherup, Robert S
|e verfasserin
|4 aut
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|a Merz, Michael
|e verfasserin
|4 aut
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|a Nagel, Peter
|e verfasserin
|4 aut
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|a Schuppler, Stefan
|e verfasserin
|4 aut
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|a Winter, Martin
|e verfasserin
|4 aut
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|a Kleiner, Karin
|e verfasserin
|4 aut
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|i Enthalten in
|t Chemistry of materials : a publication of the American Chemical Society
|d 1998
|g 35(2023), 4 vom: 28. Feb., Seite 1514-1526
|w (DE-627)NLM098194763
|x 0897-4756
|7 nnns
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| 773 |
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|g volume:35
|g year:2023
|g number:4
|g day:28
|g month:02
|g pages:1514-1526
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|u http://dx.doi.org/10.1021/acs.chemmater.2c02639
|3 Volltext
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