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231226s2023 xx |||||o 00| ||eng c |
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|a 10.1002/adma.202207130
|2 doi
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|a pubmed24n1160.xml
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|a (DE-627)NLM348193890
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|a (NLM)36305045
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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| 100 |
1 |
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|a Chumakova, Aleksandra
|e verfasserin
|4 aut
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| 245 |
1 |
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|a Multiscale Reciprocal Space Mapping of Magnetite Mesocrystals
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|c 2023
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
|b c
|2 rdamedia
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|a ƒa Online-Ressource
|b cr
|2 rdacarrier
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|a Date Completed 13.01.2023
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|a Date Revised 13.01.2023
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a © 2022 The Authors. Advanced Materials published by Wiley-VCH GmbH.
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|a Mesocrystals are a class of nanostructured material, where a multiple-length-scale structure is a prerequisite of many interesting phenomena. Resolving the mesocrystal structure is quite challenging due to their structuration on different length scales. The combination of small- and wide-angle X-ray scattering (SAXS and WAXS) techniques offers the possibility of non-destructively probing mesocrystalline structures simultaneously, over multiple length scales to reveal their microscopic structure. This work describes how high dynamical range of modern detectors sheds light on the weak features of scattering, significantly increasing the information content. The detailed analysis of X-ray diffraction (XRD) from the magnetite mesocrystals with different particle sizes and shapes is described, in tandem with electron microscopy. The revealed features provide valuable input to the models of mesocrystal growth and the choice of structural motif; the impact on magnetic properties is discussed
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|a Journal Article
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|a magnetite
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4 |
|a mesocrystals
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4 |
|a microscopic structure
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|a multiple-length-scale structures
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4 |
|a supercrystallography
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1 |
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|a Steegemans, Tristan
|e verfasserin
|4 aut
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1 |
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|a Baburin, Igor A
|e verfasserin
|4 aut
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1 |
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|a Mistonov, Alexander
|e verfasserin
|4 aut
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1 |
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|a Dubitskiy, Ilya S
|e verfasserin
|4 aut
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|a Schlotheuber, Julian
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Kirner, Felizitas
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Sturm, Sebastian
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Lubk, Axel
|e verfasserin
|4 aut
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1 |
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|a Müller-Caspary, Knut
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Wimmer, Ilona
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Fonin, Mikhail
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Sturm, Elena V
|e verfasserin
|4 aut
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| 700 |
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|a Bosak, Alexeï
|e verfasserin
|4 aut
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| 773 |
0 |
8 |
|i Enthalten in
|t Advanced materials (Deerfield Beach, Fla.)
|d 1998
|g 35(2023), 2 vom: 14. Jan., Seite e2207130
|w (DE-627)NLM098206397
|x 1521-4095
|7 nnns
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| 773 |
1 |
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|g volume:35
|g year:2023
|g number:2
|g day:14
|g month:01
|g pages:e2207130
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|u http://dx.doi.org/10.1002/adma.202207130
|3 Volltext
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