Studies on the EPR parameters and local angular distortion for the tetragonal Cu2+ center in CaWO4 crystal

© 2022 John Wiley & Sons Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 61(2023), 1 vom: 13. Jan., Seite 8-15
1. Verfasser: Chen, Baojin (VerfasserIn)
Weitere Verfasser: Yao, Linchao, Feng, Cuidi, Zhang, Huaming, Xiao, Wenbo
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2023
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article CaWO4 Cu2+ defect structures electron paramagnetic resonance (EPR)
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520 |a The electron paramagnetic resonance (EPR) parameters-g factors gi (i = || and ⊥) and hyperfine structure constants Ai (M) and Ai (N), with M and N belonging to isotopes 63 Cu2+ and 65 Cu2+ -and local structure of Cu2+ ion occupying W6+ site in CaWO4 crystal are theoretically studied based on the perturbation formulas of these parameters for a 3d9 ion under tetragonally elongated tetrahedra. In these formulas, the ligand orbital (LO) and spin-orbit coupling (SOC) contributions are included due to the shorter impurity-ligand distance R (≈1.83 Å) and hence the strong covalency of the studied [CuO4 ]6- cluster, and the related molecular orbital coefficients are quantitatively determined from the cluster approach in a uniform way; meanwhile, the required crystal field (CF) parameters for the tetragonally distorted tetrahedron (TDT) are estimated from the superposition model and the local structure of the impurity Cu2+ center. According to the calculation, the bond angle θ between the four equivalent Cu2+ -O2- bonds and the C4 axis in the CaWO4 :Cu2+ is found to be about 2.1° smaller than that (θ0  ≈ 54.74°) for an ideal tetrahedron due to the Jahn-Teller (JT) effect and the size mismatch. The fitted results agree well with the observed values, and the validity of the present assignment for the local structure of the Cu2+ center is also discussed 
650 4 |a Journal Article 
650 4 |a CaWO4 
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650 4 |a defect structures 
650 4 |a electron paramagnetic resonance (EPR) 
700 1 |a Yao, Linchao  |e verfasserin  |4 aut 
700 1 |a Feng, Cuidi  |e verfasserin  |4 aut 
700 1 |a Zhang, Huaming  |e verfasserin  |4 aut 
700 1 |a Xiao, Wenbo  |e verfasserin  |4 aut 
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