The Inner Shell Spectroscopy beamline at NSLS-II : a facility for in situ and operando X-ray absorption spectroscopy for materials research

open access.

Détails bibliographiques
Publié dans:Journal of synchrotron radiation. - 1994. - 29(2022), Pt 4 vom: 01. Juli, Seite 1095-1106
Auteur principal: Leshchev, Denis (Auteur)
Autres auteurs: Rakitin, Maksim, Luvizotto, Bruno, Kadyrov, Ruslan, Ravel, Bruce, Attenkofer, Klaus, Stavitski, Eli
Format: Article en ligne
Langue:English
Publié: 2022
Accès à la collection:Journal of synchrotron radiation
Sujets:Journal Article X-ray absorption spectroscopy beamline monochromator
Description
Résumé:open access.
The Inner Shell Spectroscopy (ISS) beamline on the 8-ID station at the National Synchrotron Light Source II (NSLS-II), Upton, NY, USA, is a high-throughput X-ray absorption spectroscopy beamline designed for in situ, operando, and time-resolved material characterization using high monochromatic flux and scanning speed. This contribution discusses the technical specifications of the beamline in terms of optics, heat load management, monochromator motion control, and data acquisition and processing. Results of the beamline tests demonstrating the quality of the data obtainable on the instrument, possible energy scanning speeds, as well as long-term beamline stability are shown. The ability to directly control the monochromator trajectory to define the acquisition time for each spectral region is highlighted. Examples of studies performed on the beamline are presented. The paper is concluded with a brief outlook for future developments
Description:Date Revised 31.08.2024
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1600-5775
DOI:10.1107/S160057752200460X