Preparation, characterization, and removal of nitrate from water using vacant polyoxometalate/TiO2 composites

Due to the rapid development of industry and agriculture, nitrate pollution in groundwater has been continuously increasing. NO3-N is a chemically stable nitrogen species and is quite difficult to remove. In this study, using heteropoly silicotungstate K8[α-SiW11O39] and Cu2+ as the active component...

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Veröffentlicht in:Environmental technology. - 1993. - 44(2023), 22 vom: 01. Sept., Seite 3393-3404
1. Verfasser: Wang, Lingsheng (VerfasserIn)
Weitere Verfasser: Fu, Weizhang, Sun, Shujuan, Liu, Huaihao, Wang, Jinhua, Zhong, Wanzhen, Ma, Bin
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2023
Zugriff auf das übergeordnete Werk:Environmental technology
Schlagworte:Journal Article Nitrate N photocatalysis titanium dioxide vacant POMs 15FIX9V2JP Nitrates polyoxometalate Water 059QF0KO0R mehr... Titanium D1JT611TNE Nitrogen N762921K75
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520 |a Due to the rapid development of industry and agriculture, nitrate pollution in groundwater has been continuously increasing. NO3-N is a chemically stable nitrogen species and is quite difficult to remove. In this study, using heteropoly silicotungstate K8[α-SiW11O39] and Cu2+ as the active components, SiW11 and Cu2+ were loaded onto TiO2 by a sol-gel method to prepare a composite photocatalyst SiW11/TiO2/Cu. The photocatalytic reduction of dissolved NO3-N was subsequently performed using SiW11/TiO2/Cu under UV irradiation, and the influence of different experimental parameters on the photocatalytic performance was investigated. The mechanism of NO3-N reduction by the composite catalyst was also investigated. Free radicals existing within the system were detected by ESR spectroscopy, and the results indicated that CO2- anion free-radicals were generated by the reaction of photogenerated holes and formic acid (HCOOH). At a SiW11/TiO2/Cu dose of 1.2 g L-1 and in the presence of HCOOH as a hole scavenger, the proposed composite catalytically reduced NO3-N anddemonstrated significantadvantages in terms of its photocatalytic activity in comparison with pure TiO2. In particular, the removal efficiency of NO3-N and the selectivity of nitrogen achieved a maximum of 96% and 77%, respectively 
650 4 |a Journal Article 
650 4 |a Nitrate N 
650 4 |a photocatalysis 
650 4 |a titanium dioxide 
650 4 |a vacant POMs 
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650 7 |a 15FIX9V2JP  |2 NLM 
650 7 |a Nitrates  |2 NLM 
650 7 |a polyoxometalate  |2 NLM 
650 7 |a Water  |2 NLM 
650 7 |a 059QF0KO0R  |2 NLM 
650 7 |a Titanium  |2 NLM 
650 7 |a D1JT611TNE  |2 NLM 
650 7 |a Nitrogen  |2 NLM 
650 7 |a N762921K75  |2 NLM 
700 1 |a Fu, Weizhang  |e verfasserin  |4 aut 
700 1 |a Sun, Shujuan  |e verfasserin  |4 aut 
700 1 |a Liu, Huaihao  |e verfasserin  |4 aut 
700 1 |a Wang, Jinhua  |e verfasserin  |4 aut 
700 1 |a Zhong, Wanzhen  |e verfasserin  |4 aut 
700 1 |a Ma, Bin  |e verfasserin  |4 aut 
773 0 8 |i Enthalten in  |t Environmental technology  |d 1993  |g 44(2023), 22 vom: 01. Sept., Seite 3393-3404  |w (DE-627)NLM098202545  |x 1479-487X  |7 nnas 
773 1 8 |g volume:44  |g year:2023  |g number:22  |g day:01  |g month:09  |g pages:3393-3404 
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