Development of recoverable adsorbents for Cr(VI) ions by grafting of a dimethylamino group-containing monomer on polyethylene substrate and subsequent quaternization

A polymeric adsorbent for removal of hexavalent chromium (Cr(VI)) ions was developed by the photografting of 2-(dimethylamino)ethyl methacrylate (DMAEMA) to a polyethylene (PE) mesh and subsequent quaternization with iodoalkanes of different alkyl chain lengths. The grafting of DMAEMA and subsequent...

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Publié dans:Environmental technology. - 1993. - 44(2023), 14 vom: 15. Juni, Seite 2025-2038
Auteur principal: Yamada, Kazunori (Auteur)
Autres auteurs: Kitao, Yoshinori, Asamoto, Hiromichi, Minamisawa, Hiroaki
Format: Article en ligne
Langue:English
Publié: 2023
Accès à la collection:Environmental technology
Sujets:Journal Article 2-(dimethylamino)ethyl methacrylate Polyethylene adsorption hexavalent chromium quaternization poly(2-(dimethylamino)ethyl methacrylate) 9002-88-4 chromium hexavalent ion 18540-29-9 plus... O0V97PV2G1 Sodium Chloride 451W47IQ8X Sodium Hydroxide 55X04QC32I Chromium 0R0008Q3JB Water Pollutants, Chemical Ions
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245 1 0 |a Development of recoverable adsorbents for Cr(VI) ions by grafting of a dimethylamino group-containing monomer on polyethylene substrate and subsequent quaternization 
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520 |a A polymeric adsorbent for removal of hexavalent chromium (Cr(VI)) ions was developed by the photografting of 2-(dimethylamino)ethyl methacrylate (DMAEMA) to a polyethylene (PE) mesh and subsequent quaternization with iodoalkanes of different alkyl chain lengths. The grafting of DMAEMA and subsequent quaternization were verified by the FT-IR and XPS measurements. The Cr(VI) ion adsorption capacity of the DMAEMA-grafted PE meshes had the maximum value at the grafted amount of 2.6 mmol/g in a 0.20 mM K2Cr2O7 solution at pH 3.0 and 30°C. The adsorption behaviour obeyed the pseudo-second order kinetic model and well expressed by Langmuir isotherm. These results suggest that the Cr(VI) ion adsorption occurs through the electrostatic interaction mainly between protonated dimethylamino groups and hydrochromate (HCrO4-) ions. The adsorption capacity of the quaternized PE-g-PDMAEMA meshes increased with an increase in the degree of quaternization and/or the alkyl chain length of the iodoalkanes used and the maximum adsorption ratio was obtained at the degree of quaternization of 54.2% for the iodoheptane-quaternized PE-g-PDMAEMA (PE-g-QC7PDMAEMA) mesh. This value was about 1.86 times higher than that of the PE-g-PDAMEMA mesh. Cr(VI) ions were successfully desorbed from the PE-g-PDMAEMA and PE-g-QC7PDMAEMA meshes in eluents such as NaOH, NaCl, and NH4Cl. In 0.50 M NaCl, 0.10 M NH4Cl, and 0.50 mM NaOH, the adsorption and desorption process was repeatedly performed without any considerable decrease and the desorption behaviour obeyed the pseudo-second order kinetic model. These results emphasise that the PE-g-PDMAEMA meshes and their quaternized products can be applied as an adsorbent for Cr(VI) ions 
650 4 |a Journal Article 
650 4 |a 2-(dimethylamino)ethyl methacrylate 
650 4 |a Polyethylene 
650 4 |a adsorption 
650 4 |a hexavalent chromium 
650 4 |a quaternization 
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650 7 |a Polyethylene  |2 NLM 
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650 7 |a chromium hexavalent ion  |2 NLM 
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650 7 |a 2-(dimethylamino)ethyl methacrylate  |2 NLM 
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650 7 |a Sodium Chloride  |2 NLM 
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650 7 |a Sodium Hydroxide  |2 NLM 
650 7 |a 55X04QC32I  |2 NLM 
650 7 |a Chromium  |2 NLM 
650 7 |a 0R0008Q3JB  |2 NLM 
650 7 |a Water Pollutants, Chemical  |2 NLM 
650 7 |a Ions  |2 NLM 
700 1 |a Kitao, Yoshinori  |e verfasserin  |4 aut 
700 1 |a Asamoto, Hiromichi  |e verfasserin  |4 aut 
700 1 |a Minamisawa, Hiroaki  |e verfasserin  |4 aut 
773 0 8 |i Enthalten in  |t Environmental technology  |d 1993  |g 44(2023), 14 vom: 15. Juni, Seite 2025-2038  |w (DE-627)NLM098202545  |x 1479-487X  |7 nnas 
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856 4 0 |u http://dx.doi.org/10.1080/09593330.2021.2020339  |3 Volltext 
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