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231225s2021 xx |||||o 00| ||eng c |
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|a 10.1016/j.pnmrs.2021.04.002
|2 doi
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|a pubmed25n1112.xml
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|a (PII)S0079-6565(21)00015-7
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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| 100 |
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|a Elliott, Stuart J
|e verfasserin
|4 aut
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| 245 |
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|a Practical dissolution dynamic nuclear polarization
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|c 2021
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| 336 |
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|a Text
|b txt
|2 rdacontent
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| 337 |
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|a ƒaComputermedien
|b c
|2 rdamedia
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| 338 |
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|a ƒa Online-Ressource
|b cr
|2 rdacarrier
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| 500 |
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|a Date Completed 27.01.2022
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|a Date Revised 27.01.2022
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|a published: Print-Electronic
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|a Citation Status MEDLINE
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|a Copyright © 2021 Elsevier B.V. All rights reserved.
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|a This review article intends to provide insightful advice for dissolution-dynamic nuclear polarization in the form of a practical handbook. The goal is to aid research groups to effectively perform such experiments in their own laboratories. Previous review articles on this subject have covered a large number of useful topics including instrumentation, experimentation, theory, etc. The topics to be addressed here will include tips for sample preparation and for checking sample health; a checklist to correctly diagnose system faults and perform general maintenance; the necessary mechanical requirements regarding sample dissolution; and aids for accurate, fast and reliable polarization quantification. Herein, the challenges and limitations of each stage of a typical dissolution-dynamic nuclear polarization experiment are presented, with the focus being on how to quickly and simply overcome some of the limitations often encountered in the laboratory
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|a Journal Article
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|a Research Support, Non-U.S. Gov't
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|a Review
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4 |
|a CP
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| 650 |
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4 |
|a DNP
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| 650 |
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|a Hyperpolarization
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| 650 |
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|a NMR
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|a Polarization quantification
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|a SPY-NMR
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|a Sample preparation
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| 650 |
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|a Systems maintenance
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| 650 |
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|a Transport dynamics
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|a dDNP
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1 |
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|a Stern, Quentin
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Ceillier, Morgan
|e verfasserin
|4 aut
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| 700 |
1 |
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|a El Daraï, Théo
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Cousin, Samuel F
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Cala, Olivier
|e verfasserin
|4 aut
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| 700 |
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|a Jannin, Sami
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Progress in nuclear magnetic resonance spectroscopy
|d 1998
|g 126-127(2021) vom: 01. Okt., Seite 59-100
|w (DE-627)NLM098212745
|x 1873-3301
|7 nnas
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| 773 |
1 |
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|g volume:126-127
|g year:2021
|g day:01
|g month:10
|g pages:59-100
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|u http://dx.doi.org/10.1016/j.pnmrs.2021.04.002
|3 Volltext
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