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231225s2022 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.5215
|2 doi
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|a pubmed24n1100.xml
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|a eng
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|a Crouch, Ronald C
|e verfasserin
|4 aut
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|a 19 F-detected dual-optimized inverted 1 JCC 1,n-ADEQUATE
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|c 2022
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|a Text
|b txt
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|a ƒaComputermedien
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|a ƒa Online-Ressource
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|a Date Completed 04.03.2022
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|a Date Revised 04.03.2022
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a © 2021 John Wiley & Sons, Ltd.
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|a Modification of the recently reported 19 F-detected 1,1-ADEQUATE experiment that incorporates dual-optimization to selectively invert a wide range of 1 JCC correlations in a 1,n-ADEQUATE experiment is reported. Parameters for the dual-optimization segment of the pulse sequence were modified to accommodate the increased size of 1 JCC homonuclear coupling constants of poly- and perfluorinated molecules relative to protonated molecules to allow broadband inversion of the 1 JCC correlations. The observation and utility of isotope shifts are reported for the first time for 1,1- and 1,n-ADEQUATE correlations
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|a Journal Article
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|a 1,1-ADEQUATE
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|a 1,n-ADEQUATE
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|a 19F-detection
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|a dual-optimization
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| 650 |
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|a isotope shifts
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1 |
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|a Raab, Jeffrey G
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Pelmuş, Marius
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Tischenko, Evgeny
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Frey, Michael
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Buevich, Alexei V
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Reibarkh, Mikhail
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Williamson, R Thomas
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Martin, Gary E
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 60(2022), 2 vom: 25. Feb., Seite 210-220
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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| 773 |
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|g volume:60
|g year:2022
|g number:2
|g day:25
|g month:02
|g pages:210-220
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|u http://dx.doi.org/10.1002/mrc.5215
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