Complete 1 H and 13 C NMR spectral assignment of venturicidin A by 2D NMR spectroscopy
Copyright © 1989 John Wiley & Sons, Ltd.
| Publié dans: | Magnetic resonance in chemistry : MRC. - 1985. - 27(1989), 9 vom: 25. Sept., Seite 863-871 |
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| Auteur principal: | |
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| Format: | Article en ligne |
| Langue: | English |
| Publié: |
1989
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| Accès à la collection: | Magnetic resonance in chemistry : MRC |
| Sujets: | Journal Article COLOC-S COSY Long-range CH correlation NOESY One-bond CH correlation Selective INEPT |
| Résumé: | Copyright © 1989 John Wiley & Sons, Ltd. After correlation of the majority of signals by COSY and one-bond heteronuclear correlation, the complete assignment of the 1 H and 13 C NMR spectra of the macrolide antibiotic venturicidin A required the application of long-range CH coupling information. This was accessible by the COLOC-S and selective INEPT experiments, and the sensitivity of these experiments is discussed. Steric information was obtained from a NOESY spectrum, and the solution structure compared with that in the crystal |
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| Description: | Date Revised 26.05.2021 published: Print Citation Status PubMed-not-MEDLINE |
| ISSN: | 1097-458X |
| DOI: | 10.1002/mrc.1260270909 |