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|a 10.1107/S160057752100103X
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|a pubmed24n1073.xml
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|a (DE-627)NLM32208184X
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|a (NLM)33650575
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|a DE-627
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|a eng
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|a Zhu, Suyun
|e verfasserin
|4 aut
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|a HIPPIE
|b a new platform for ambient-pressure X-ray photoelectron spectroscopy at the MAX IV Laboratory
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|c 2021
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|a Text
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|a Date Revised 08.04.2021
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a open access.
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|a HIPPIE is a soft X-ray beamline on the 3 GeV electron storage ring of the MAX IV Laboratory, equipped with a novel ambient-pressure X-ray photoelectron spectroscopy (APXPS) instrument. The endstation is dedicated to performing in situ and operando X-ray photoelectron spectroscopy experiments in the presence of a controlled gaseous atmosphere at pressures up to 30 mbar [1 mbar = 100 Pa] as well as under ultra-high-vacuum conditions. The photon energy range is 250 to 2200 eV in planar polarization and with photon fluxes >1012 photons s-1 (500 mA ring current) at a resolving power of greater than 10000 and up to a maximum of 32000. The endstation currently provides two sample environments: a catalysis cell and an electrochemical/liquid cell. The former allows APXPS measurements of solid samples in the presence of a gaseous atmosphere (with a mixture of up to eight gases and a vapour of a liquid) and simultaneous analysis of the inlet/outlet gas composition by online mass spectrometry. The latter is a more versatile setup primarily designed for APXPS at the solid-liquid (dip-and-pull setup) or liquid-gas (liquid microjet) interfaces under full electrochemical control, and it can also be used as an open port for ad hoc-designed non-standard APXPS experiments with different sample environments. The catalysis cell can be further equipped with an IR reflection-absorption spectrometer, allowing for simultaneous APXPS and IR spectroscopy of the samples. The endstation is set up to easily accommodate further sample environments
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|a Journal Article
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|a APXPS
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|a IR
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|a beamline
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|a catalysis
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|a in situ
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|a operando
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|a synchrotron
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|a Scardamaglia, Mattia
|e verfasserin
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|a Kundsen, Jan
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|a Sankari, Rami
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|a Tarawneh, Hamed
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|a Temperton, Robert
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|a Pickworth, Louisa
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|a Cavalca, Filippo
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|a Wang, Chunlei
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|a Tissot, Héloïse
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|a Weissenrieder, Jonas
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|a Hagman, Benjamin
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|a Gustafson, Johan
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|a Kaya, Sarp
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|a Lindgren, Fredrik
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|a Källquist, Ida
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|a Maibach, Julia
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|a Hahlin, Maria
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|a Boix, Virginia
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|a Gallo, Tamires
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|a Rehman, Foqia
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|a D'Acunto, Giulio
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|a Schnadt, Joachim
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|a Shavorskiy, Andrey
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|i Enthalten in
|t Journal of synchrotron radiation
|d 1994
|g 28(2021), Pt 2 vom: 01. März, Seite 624-636
|w (DE-627)NLM09824129X
|x 1600-5775
|7 nnns
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|g volume:28
|g year:2021
|g number:Pt 2
|g day:01
|g month:03
|g pages:624-636
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|u http://dx.doi.org/10.1107/S160057752100103X
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