Multi-analyser detector (MAD) for high-resolution and high-energy powder X-ray diffraction

Multi-analyser detector (MAD) for high-resolution and high-energy powder X-ray diffraction

open access.

Bibliographische Detailangaben
Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 28(2021), Pt 1 vom: 01. Jan., Seite 146-157
1. Verfasser: Schökel, Alexander (VerfasserIn)
Weitere Verfasser: Etter, Martin, Berghäuser, Andreas, Horst, Alexander, Lindackers, Dirk, Whittle, Thomas A, Schmid, Siegbert, Acosta, Matias, Knapp, Michael, Ehrenberg, Helmut, Hinterstein, Manuel
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2021
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article BZT–xBCT high-energy diffraction high-resolution detectors multi-analyser detectors powder X-ray diffraction strontium niobate titanate strontium niobate zirconate
Beschreibung
Zusammenfassung:open access.
For high-resolution powder diffraction in material science, high photon energies are necessary, especially for in situ and in operando experiments. For this purpose, a multi-analyser detector (MAD) was developed for the high-energy beamline P02.1 at PETRA III of the Deutsches Elektronen-Synchrotron (DESY). In order to be able to adjust the detector for the high photon energies of 60 keV, an individually adjustable analyser-crystal setup was designed. The adjustment is performed via piezo stepper motors for each of the ten channels. The detector shows a low and flat background as well as a high signal-to-noise ratio. A range of standard materials were measured for characterizing the performance. Two exemplary experiments were performed to demonstrate the potential for sophisticated structural analysis with the MAD: (i) the structure of a complex material based on strontium niobate titanate and strontium niobate zirconate was determined and (ii) an in situ stroboscopy experiment with an applied electric field on a highly absorbing piezoceramic was performed. These experiments demonstrate the capabilities of the new MAD, which advances the frontiers of the structural characterization of materials
Beschreibung:Date Revised 06.10.2024
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1600-5775
DOI:10.1107/S1600577520013223