A portable on-axis laser-heating system for near-90° X-ray spectroscopy : application to ferropericlase and iron silicide

open access.

Bibliographische Detailangaben
Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 27(2020), Pt 2 vom: 01. März, Seite 414-424
1. Verfasser: Spiekermann, Georg (VerfasserIn)
Weitere Verfasser: Kupenko, Ilya, Petitgirard, Sylvain, Harder, Manuel, Nyrow, Alexander, Weis, Christopher, Albers, Christian, Biedermann, Nicole, Libon, Lélia, Sahle, Christoph J, Cerantola, Valerio, Glazyrin, Konstantin, Konôpková, Zuzana, Sinmyo, Ryosuke, Morgenroth, Wolfgang, Sergueev, Ilya, Yavaş, Hasan, Dubrovinsky, Leonid, Tolan, Metin, Sternemann, Christian, Wilke, Max
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2020
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article X-ray emission spectroscopy extreme conditions high pressure laser heating nuclear resonant inelastic scattering
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520 |a A portable IR fiber laser-heating system, optimized for X-ray emission spectroscopy (XES) and nuclear inelastic scattering (NIS) spectroscopy with signal collection through the radial opening of diamond anvil cells near 90°with respect to the incident X-ray beam, is presented. The system offers double-sided on-axis heating by a single laser source and zero attenuation of incoming X-rays other than by the high-pressure environment. A description of the system, which has been tested for pressures above 100 GPa and temperatures up to 3000 K, is given. The XES spectra of laser-heated Mg0.67Fe0.33O demonstrate the potential to map the iron spin state in the pressure-temperature range of the Earth's lower mantle, and the NIS spectra of laser-heated FeSi give access to the sound velocity of this candidate of a phase inside the Earth's core. This portable system represents one of the few bridges across the gap between laser heating and high-resolution X-ray spectroscopies with signal collection near 90° 
650 4 |a Journal Article 
650 4 |a X-ray emission spectroscopy 
650 4 |a extreme conditions 
650 4 |a high pressure 
650 4 |a laser heating 
650 4 |a nuclear resonant inelastic scattering 
700 1 |a Kupenko, Ilya  |e verfasserin  |4 aut 
700 1 |a Petitgirard, Sylvain  |e verfasserin  |4 aut 
700 1 |a Harder, Manuel  |e verfasserin  |4 aut 
700 1 |a Nyrow, Alexander  |e verfasserin  |4 aut 
700 1 |a Weis, Christopher  |e verfasserin  |4 aut 
700 1 |a Albers, Christian  |e verfasserin  |4 aut 
700 1 |a Biedermann, Nicole  |e verfasserin  |4 aut 
700 1 |a Libon, Lélia  |e verfasserin  |4 aut 
700 1 |a Sahle, Christoph J  |e verfasserin  |4 aut 
700 1 |a Cerantola, Valerio  |e verfasserin  |4 aut 
700 1 |a Glazyrin, Konstantin  |e verfasserin  |4 aut 
700 1 |a Konôpková, Zuzana  |e verfasserin  |4 aut 
700 1 |a Sinmyo, Ryosuke  |e verfasserin  |4 aut 
700 1 |a Morgenroth, Wolfgang  |e verfasserin  |4 aut 
700 1 |a Sergueev, Ilya  |e verfasserin  |4 aut 
700 1 |a Yavaş, Hasan  |e verfasserin  |4 aut 
700 1 |a Dubrovinsky, Leonid  |e verfasserin  |4 aut 
700 1 |a Tolan, Metin  |e verfasserin  |4 aut 
700 1 |a Sternemann, Christian  |e verfasserin  |4 aut 
700 1 |a Wilke, Max  |e verfasserin  |4 aut 
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