Design and performance of a new setup for spatially resolved transmission X-ray photoelectron spectroscopy at the Swiss Light Source

open access.

Bibliographische Detailangaben
Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 26(2019), Pt 3 vom: 01. Mai, Seite 785-792
1. Verfasser: Roy, Kanak (VerfasserIn)
Weitere Verfasser: Raabe, Joerg, Schifferle, Pascal, Finizio, Simone, Kleibert, Armin, van Bokhoven, Jeroen A, Artiglia, Luca
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2019
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article X-ray photoelectron spectroscopy X-ray spectromicroscopy scanning transmission X-ray microscope spatial resolution
LEADER 01000caa a22002652 4500
001 NLM296936154
003 DE-627
005 20240720232057.0
007 cr uuu---uuuuu
008 231225s2019 xx |||||o 00| ||eng c
024 7 |a 10.1107/S1600577519002984  |2 doi 
028 5 2 |a pubmed24n1476.xml 
035 |a (DE-627)NLM296936154 
035 |a (NLM)31074443 
040 |a DE-627  |b ger  |c DE-627  |e rakwb 
041 |a eng 
100 1 |a Roy, Kanak  |e verfasserin  |4 aut 
245 1 0 |a Design and performance of a new setup for spatially resolved transmission X-ray photoelectron spectroscopy at the Swiss Light Source 
264 1 |c 2019 
336 |a Text  |b txt  |2 rdacontent 
337 |a ƒaComputermedien  |b c  |2 rdamedia 
338 |a ƒa Online-Ressource  |b cr  |2 rdacarrier 
500 |a Date Revised 20.07.2024 
500 |a published: Print-Electronic 
500 |a Citation Status PubMed-not-MEDLINE 
520 |a open access. 
520 |a The successful design, installation and operation of a high spatial resolution X-ray photoelectron spectrometer at the Swiss Light Source is presented. In this instrument, a Fresnel zone plate is used to focus an X-ray beam onto the sample and an electron analyzer positioned at 45° with respect to the incoming beam direction is used to collect photoelectrons from the backside of the sample. By raster scanning the sample, transmitted current, X-ray absorption and X-ray photoemission maps can be simultaneously acquired. This work demonstrates that chemical information can be extracted with micrometre resolution; the results suggest that a spatial resolution better than 100 nm can be achieved with this approach in future. This kind of photoelectron spectromicroscope will allow in situ measurements with high spatial resolution also under ambient pressure conditions (in the millibar range). Element-specific X-ray photoemission maps can be obtained before and while exposing the sample to gas/gas mixtures to show morphological and chemical changes of the surface 
650 4 |a Journal Article 
650 4 |a X-ray photoelectron spectroscopy 
650 4 |a X-ray spectromicroscopy 
650 4 |a scanning transmission X-ray microscope 
650 4 |a spatial resolution 
700 1 |a Raabe, Joerg  |e verfasserin  |4 aut 
700 1 |a Schifferle, Pascal  |e verfasserin  |4 aut 
700 1 |a Finizio, Simone  |e verfasserin  |4 aut 
700 1 |a Kleibert, Armin  |e verfasserin  |4 aut 
700 1 |a van Bokhoven, Jeroen A  |e verfasserin  |4 aut 
700 1 |a Artiglia, Luca  |e verfasserin  |4 aut 
773 0 8 |i Enthalten in  |t Journal of synchrotron radiation  |d 1994  |g 26(2019), Pt 3 vom: 01. Mai, Seite 785-792  |w (DE-627)NLM09824129X  |x 1600-5775  |7 nnns 
773 1 8 |g volume:26  |g year:2019  |g number:Pt 3  |g day:01  |g month:05  |g pages:785-792 
856 4 0 |u http://dx.doi.org/10.1107/S1600577519002984  |3 Volltext 
912 |a GBV_USEFLAG_A 
912 |a SYSFLAG_A 
912 |a GBV_NLM 
912 |a GBV_ILN_40 
912 |a GBV_ILN_350 
912 |a GBV_ILN_2005 
951 |a AR 
952 |d 26  |j 2019  |e Pt 3  |b 01  |c 05  |h 785-792