A high-throughput energy-dispersive tender X-ray spectrometer for shot-to-shot sulfur measurements

open access.

Bibliographische Detailangaben
Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 26(2019), Pt 3 vom: 01. Mai, Seite 629-634
1. Verfasser: Abraham, Baxter (VerfasserIn)
Weitere Verfasser: Nowak, Stanislaw, Weninger, Clemens, Armenta, Rebecca, Defever, Jim, Day, David, Carini, Gabriella, Nakahara, Kazutaka, Gallo, Alessandro, Nelson, Silke, Nordlund, Dennis, Kroll, Thomas, Hunter, Mark S, van Driel, Tim, Zhu, Diling, Weng, Tsu Chien, Alonso-Mori, Roberto, Sokaras, Dimosthenis
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2019
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article X-ray absorption spectroscopy X-ray emission spectroscopy X-ray free-electron lasers photon-in photon-out spectroscopy methods tender X-rays
Beschreibung
Zusammenfassung:open access.
An X-ray emission spectrometer that can detect the sulfur Kα emission lines with large throughput and a high energy resolution is presented. The instrument is based on a large d-spacing perfect Bragg analyzer that diffracts the sulfur Kα emission at close to backscattering angles. This facilitates the application of efficient concepts routinely employed in hard X-ray spectrometers towards the tender X-ray regime. The instrument described in this work is based on an energy-dispersive von Hamos geometry that is well suited for photon-in photon-out spectroscopy at X-ray free-electron laser and synchrotron sources. Comparison of its performance with previously used instrumentation is presented through measurements using sulfur-containing species performed at the LCLS. It is shown that the overall signal intensity is increased by a factor of ∼15. Implementation of this approach in the design of a tender X-ray spectroscopy endstation for LCLS-II is also discussed
Beschreibung:Date Revised 20.07.2024
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1600-5775
DOI:10.1107/S1600577519002431