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231225s2019 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.4844
|2 doi
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|a pubmed24n0977.xml
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|a eng
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|a Ahmed, Raheel
|e verfasserin
|4 aut
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|a 1 H-13 C HMBC NMR experiments as a structural and analytical tool for the characterization of elusive trans/cis hydroperoxide isomers from oxidized unsaturated fatty acids in solution
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|c 2019
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|2 rdacarrier
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|a Date Completed 16.09.2019
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|a Date Revised 16.09.2019
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a © 2019 John Wiley & Sons, Ltd.
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|a The radical-dependent oxidation of unsaturated fatty acids is a fundamental reaction in lipid chemistry, biochemistry, and technology. We report herein the first successful application of 1 H-13 C HMBC NMR experiment for the identification and quantification of complex and minor (3.9% to 0.85%) components of cis and trans primary hydroperoxide isomers of oxidized oleate and linoleate methyl esters in solution, without the need of laborious isolation of the individual components
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|a Journal Article
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|a 1H-13C HMBC
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|a NMR
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|a chemical shifts
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|a coupling constants
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|a hydroperoxides
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| 650 |
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4 |
|a unsaturated lipids
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1 |
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|a Siddiqui, Hina
|e verfasserin
|4 aut
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1 |
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|a Choudhary, Muhammad Iqbal
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Gerothanassis, Ioannis P
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 57(2019), 4 vom: 15. Apr., Seite S69-S74
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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|g volume:57
|g year:2019
|g number:4
|g day:15
|g month:04
|g pages:S69-S74
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|u http://dx.doi.org/10.1002/mrc.4844
|3 Volltext
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