Development of a new vacuum impregnation method at room atmosphere to produce silver-copper oxide nanoparticles on activated carbon for antibacterial applications

A new impregnation method was tested in this study. Without a stabilizing agent, silver and copper metallic compounds were directly impregnated on activated carbon using vacuum impregnation followed by drying at 100°C and vacuum impregnation followed by thermal decomposition at 350°C in an ambient a...

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Veröffentlicht in:Environmental technology. - 1993. - 41(2020), 18 vom: 04. Juli, Seite 2400-2411
1. Verfasser: Arakawa, Flávia Sayuri (VerfasserIn)
Weitere Verfasser: Shimabuku-Biadola, Quelen Letícia, Fernandes Silva, Marcela, Bergamasco, Rosangela
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2020
Zugriff auf das übergeordnete Werk:Environmental technology
Schlagworte:Journal Article Escherichia coli Characterization metal nanoparticles modification thermal decomposition Anti-Bacterial Agents Oxides Charcoal 16291-96-6 mehr... Silver 3M4G523W1G Copper 789U1901C5
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245 1 0 |a Development of a new vacuum impregnation method at room atmosphere to produce silver-copper oxide nanoparticles on activated carbon for antibacterial applications 
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520 |a A new impregnation method was tested in this study. Without a stabilizing agent, silver and copper metallic compounds were directly impregnated on activated carbon using vacuum impregnation followed by drying at 100°C and vacuum impregnation followed by thermal decomposition at 350°C in an ambient atmosphere. The effect of thermal decomposition on the structural, morphological, and textural characteristics of the modified nanomaterials was analysed by Brunauer-Emmett-Teller, X-ray diffraction, scanning electron microscopy, energy dispersive X-Ray, and transmission electron microscopy. The characteristics of the produced materials were not altered. Silver and CuO nanoparticles were identified in the samples with average diameters ranging from 33.3-36.8 nm and 29.0-33.3 nm, respectively. The materials were tested for their antibacterial capacity and for their potential to leach Ag and Cu into water, thus analysing the effect of the thermal decomposition process on the impregnation process. The vacuum impregnation process followed by thermal decomposition produced the best results, with the resultant material reducing bacterial abundance by 5.31-6.61 log and leaching only low concentrations of metals into the water (Ag - 0.010-0.025 mg L-1 and Cu - 0.270-0.361 mg L-1). Samples produced without the thermal decomposition step reached bacterial reductions of 1.86-1.97 log and yielded higher concentrations of metals in the water (Ag - 0.051-0.086 mg L-1 and Cu - 0.819-0.894 mg L-1) 
650 4 |a Journal Article 
650 4 |a Escherichia coli 
650 4 |a Characterization 
650 4 |a metal nanoparticles 
650 4 |a modification 
650 4 |a thermal decomposition 
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650 7 |a Oxides  |2 NLM 
650 7 |a Charcoal  |2 NLM 
650 7 |a 16291-96-6  |2 NLM 
650 7 |a Silver  |2 NLM 
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700 1 |a Shimabuku-Biadola, Quelen Letícia  |e verfasserin  |4 aut 
700 1 |a Fernandes Silva, Marcela  |e verfasserin  |4 aut 
700 1 |a Bergamasco, Rosangela  |e verfasserin  |4 aut 
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773 1 8 |g volume:41  |g year:2020  |g number:18  |g day:04  |g month:07  |g pages:2400-2411 
856 4 0 |u http://dx.doi.org/10.1080/09593330.2019.1567607  |3 Volltext 
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