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231225s2018 xx |||||o 00| ||eng c |
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|a 10.1021/acs.langmuir.8b01114
|2 doi
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|a pubmed24n0952.xml
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|a (DE-627)NLM285831836
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|a (NLM)29939748
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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|a Ishizaki, Yuya
|e verfasserin
|4 aut
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|a Synthesis and Porous SiO2 Nanofilm Formation of the Silsesquioxane-Containing Amphiphilic Block Copolymer
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|c 2018
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|2 rdacarrier
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|a Date Completed 24.09.2018
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|a Date Revised 24.09.2018
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a We describe the synthesis, Langmuir-Blodgett (LB) film formation, and photo-oxidation of an organic-inorganic hybrid block copolymer consisting of N-dodecyl acrylamide (DDA) and silsesquioxane (SQ) comonomers [p(DDA/SQ26)- b-pDDA]. The copolymer was synthesized by reversible addition fragmentation chain transfer polymerization of DDA and SQ. Higher monolayer stability at the air-water interface was confirmed for p(DDA/SQ26)- b-pDDA. The p(DDA/SQ26)- b-pDDA monolayer was deposited onto solid substrates with a monolayer thickness of 2.3 nm. The photo-oxidized SiO2 nanofilm revealed its porous structure, which reflects phase-separated structures of p(DDA/SQ26)- b-pDDA, as confirmed using atomic force microscopy, quartz crystal microbalance, and cyclic voltammetry measurements. These results demonstrate that this preparation method using photo-oxidation of the organic-inorganic hybrid block copolymer LB film is promising for manipulating pore formations of inorganic oxide nanofilms
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|a Journal Article
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|a Research Support, Non-U.S. Gov't
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|a Yamamoto, Shunsuke
|e verfasserin
|4 aut
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|a Miyashita, Tokuji
|e verfasserin
|4 aut
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|a Mitsuishi, Masaya
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Langmuir : the ACS journal of surfaces and colloids
|d 1992
|g 34(2018), 27 vom: 10. Juli, Seite 8007-8014
|w (DE-627)NLM098181009
|x 1520-5827
|7 nnns
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|g volume:34
|g year:2018
|g number:27
|g day:10
|g month:07
|g pages:8007-8014
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|u http://dx.doi.org/10.1021/acs.langmuir.8b01114
|3 Volltext
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