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231224s2017 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.4584
|2 doi
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|a pubmed24n0896.xml
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|a eng
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| 100 |
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|a Kupče, Ēriks
|e verfasserin
|4 aut
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|a 2BOB - extracting an H2BC and an HSQC-type spectrum from the same data set, and H2OBC - a fast experiment delineating the protonated 13 C backbone
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|c 2017
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|2 rdacarrier
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|a Date Completed 05.03.2018
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|a Date Revised 05.03.2018
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a Copyright © 2017 John Wiley & Sons, Ltd.
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|a Two new related methods, 2BOB and H2OBC, for tracking out the backbone of protonated 13 C nuclei are presented. 2BOB extracts an H2BC and an HSQC-type spectrum from one and the same data set, and the combined information of these two spectra tracks out the molecular backbone. The faster method, H2OBC, typically requiring only a few minutes of instrument time, yields a single spectrum with distinct and different phases imposed on the H2BC and one-bond peaks thus obviating the need to separate them in the absence of complicating spectral overlap. Copyright © 2017 John Wiley & Sons, Ltd
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|a Journal Article
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|a 2BOB
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|a COSY
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|a H2BC
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|a H2OBC
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| 650 |
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|a HMQC
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|a HSQC
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|a quinine
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|a structure elucidation
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| 650 |
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|a tobramycin
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1 |
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|a Sørensen, Ole W
|e verfasserin
|4 aut
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 55(2017), 6 vom: 30. Juni, Seite 515-518
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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| 773 |
1 |
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|g volume:55
|g year:2017
|g number:6
|g day:30
|g month:06
|g pages:515-518
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|u http://dx.doi.org/10.1002/mrc.4584
|3 Volltext
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