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231224s2016 xx ||||| 00| ||eng c |
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|a pubmed25n0884.xml
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|a (DE-627)NLM265286468
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|a (NLM)27738414
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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1 |
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|a Vergentev, Tikhon
|e verfasserin
|4 aut
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|a A rapid two-dimensional data collection system for the study of ferroelectric materials under external applied electric fields
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|c 2016
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Revised 30.09.2020
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|a published: Electronic-eCollection
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|a Citation Status PubMed-not-MEDLINE
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|a Synchrotron X-rays on the Swiss Norwegian Beamline and BM28 (XMaS) at the ESRF have been used to record the diffraction response of the PMN-PT relaxor piezoelectric 67% Pb(Mg1/3Nb2/3)O3-33% PbTiO3 as a function of externally applied electric field. A DC field in the range 0-18 kV cm-1 was applied along the [001] pseudo-cubic direction using a specially designed sample cell for in situ single-crystal diffraction experiments. The cell allowed data to be collected on a Pilatus 2M area detector in a large volume of reciprocal space using transmission geometry. The data showed good agreement with a twinned single-phase monoclinic structure model. The results from the area detector were compared with previous Bragg peak mapping using variable electric fields and a single detector where the structural model was ambiguous. The coverage of a significantly larger section of reciprocal space facilitated by the area detector allowed precise phase analysis
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|a Journal Article
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|a PMN-PT
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|a area detectors
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|a diffuse scattering
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|a ferroelectricity
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|a in situ two-dimensional X-ray single-crystal diffraction
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|a phase transitions
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|a piezoelectricity
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|a synchrotron X-rays
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|a Bronwald, Iurii
|e verfasserin
|4 aut
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|a Chernyshov, Dmitry
|e verfasserin
|4 aut
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|a Gorfman, Semen
|e verfasserin
|4 aut
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|a Ryding, Stephanie H M
|e verfasserin
|4 aut
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|a Thompson, Paul
|e verfasserin
|4 aut
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|a Cernik, Robert J
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Journal of applied crystallography
|d 1998
|g 49(2016), Pt 5 vom: 01. Okt., Seite 1501-1507
|w (DE-627)NLM098121561
|x 0021-8898
|7 nnns
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| 773 |
1 |
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|g volume:49
|g year:2016
|g number:Pt 5
|g day:01
|g month:10
|g pages:1501-1507
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|a GBV_USEFLAG_A
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|a SYSFLAG_A
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|a GBV_NLM
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|a GBV_ILN_350
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|a AR
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|d 49
|j 2016
|e Pt 5
|b 01
|c 10
|h 1501-1507
|