Utilizing broadband X-rays in a Bragg coherent X-ray diffraction imaging experiment

A method is presented to simplify Bragg coherent X-ray diffraction imaging studies of complex heterogeneous crystalline materials with a two-stage screening/imaging process that utilizes polychromatic and monochromatic coherent X-rays and is compatible with in situ sample environments. Coherent whit...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 23(2016), Pt 5 vom: 01. Sept., Seite 1241-4
1. Verfasser: Cha, Wonsuk (VerfasserIn)
Weitere Verfasser: Liu, Wenjun, Harder, Ross, Xu, Ruqing, Fuoss, Paul H, Hruszkewycz, Stephan O
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2016
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article Research Support, U.S. Gov't, Non-P.H.S. coherent X-ray diffraction imaging materials characterization polychromatic X-ray diffraction
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520 |a A method is presented to simplify Bragg coherent X-ray diffraction imaging studies of complex heterogeneous crystalline materials with a two-stage screening/imaging process that utilizes polychromatic and monochromatic coherent X-rays and is compatible with in situ sample environments. Coherent white-beam diffraction is used to identify an individual crystal particle or grain that displays desired properties within a larger population. A three-dimensional reciprocal-space map suitable for diffraction imaging is then measured for the Bragg peak of interest using a monochromatic beam energy scan that requires no sample motion, thus simplifying in situ chamber design. This approach was demonstrated with Au nanoparticles and will enable, for example, individual grains in a polycrystalline material of specific orientation to be selected, then imaged in three dimensions while under load 
650 4 |a Journal Article 
650 4 |a Research Support, U.S. Gov't, Non-P.H.S. 
650 4 |a coherent X-ray diffraction imaging 
650 4 |a materials characterization 
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700 1 |a Liu, Wenjun  |e verfasserin  |4 aut 
700 1 |a Harder, Ross  |e verfasserin  |4 aut 
700 1 |a Xu, Ruqing  |e verfasserin  |4 aut 
700 1 |a Fuoss, Paul H  |e verfasserin  |4 aut 
700 1 |a Hruszkewycz, Stephan O  |e verfasserin  |4 aut 
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