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231224s2017 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.4322
|2 doi
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|a pubmed25n0841.xml
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|a (NLM)26332452
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|a DE-627
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|a eng
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|a Saurí, Josep
|e verfasserin
|4 aut
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|a Improving the performance of J-modulated ADEQUATE experiments through homonuclear decoupling and non-uniform sampling
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|c 2017
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|a Date Completed 17.04.2018
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|a Date Revised 17.04.2018
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|a published: Print-Electronic
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|a Citation Status MEDLINE
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|a Copyright © 2015 John Wiley & Sons, Ltd.
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|a Homonuclear 13 C-13 C couplings at natural abundance can be measured using the J-modulated Adequate DoublE QUAntumTransfer Experiment (ADEQUATE) experiment. To somewhat ameliorate F1 digitization requirements, a scaling factor was incorporated into the original pulse sequence. Non-uniform sampling provides an obvious avenue to further facilitate the acquisition of 1 JCC and n JCC homonuclear coupling constant data. We introduce homonuclear decoupling (HD) analogous to that described for the 1,1-HD-ADEQUATE and 1,n-HD-ADEQUATE experiments and evaluate the combination of non-uniform sampling and HD on the acquisition of both 1 JCC and n JCC homonuclear 13 C-13 C coupling constants using ibuprofen as a model compound. Copyright © 2015 John Wiley & Sons, Ltd
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|a Journal Article
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|a 13C-13C homonuclear coupling constants
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|a ADEQUATE
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|a J-modulated ADEQUATE
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|a broadband homonuclear decoupling
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|a non-uniform sampling (NUS)
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| 650 |
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|a Carbon Isotopes
|2 NLM
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| 650 |
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|a Ibuprofen
|2 NLM
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| 650 |
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|a WK2XYI10QM
|2 NLM
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| 700 |
1 |
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|a Parella, Teodor
|e verfasserin
|4 aut
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1 |
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|a Williamson, R Thomas
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Martin, Gary E
|e verfasserin
|4 aut
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 55(2017), 3 vom: 07. März, Seite 191-197
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnas
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| 773 |
1 |
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|g volume:55
|g year:2017
|g number:3
|g day:07
|g month:03
|g pages:191-197
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|u http://dx.doi.org/10.1002/mrc.4322
|3 Volltext
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|d 55
|j 2017
|e 3
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|h 191-197
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