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231224s2016 xx |||||o 00| ||eng c |
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|a 10.1002/mrc.4259
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|a eng
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|a Foley, David A
|e verfasserin
|4 aut
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|a Reaction monitoring using online vs tube NMR spectroscopy
|b seriously different results
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|c 2016
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|a Text
|b txt
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|a Date Completed 24.01.2018
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|a Date Revised 24.01.2018
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a Copyright © 2015 John Wiley & Sons, Ltd.
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|a We report findings from the qualitative evaluation of nuclear magnetic resonance (NMR) reaction monitoring techniques of how each relates to the kinetic profile of a reaction process. The study highlights key reaction rate differences observed between the various NMR reaction monitoring methods investigated: online NMR, static NMR tubes, and periodic inversion of NMR tubes. The analysis of three reaction processes reveals that rates derived from NMR analysis are highly dependent on monitoring method. These findings indicate that users must be aware of the effect of their monitoring method upon the kinetic rate data derived from NMR analysis. Copyright © 2015 John Wiley & Sons, Ltd
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|a Journal Article
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|a NMR reaction monitoring
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|a online NMR
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|a reaction mechanism
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| 700 |
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|a Dunn, Anna L
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Zell, Mark T
|e verfasserin
|4 aut
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 54(2016), 6 vom: 04. Juni, Seite 451-6
|w (DE-627)NLM098179667
|x 1097-458X
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|g volume:54
|g year:2016
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|g day:04
|g month:06
|g pages:451-6
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|u http://dx.doi.org/10.1002/mrc.4259
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