In situ hydrogen loading on zirconium powder

For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 22(2015), 4 vom: 02. Juli, Seite 995-1000
1. Verfasser: Maimaitiyili, Tuerdi (VerfasserIn)
Weitere Verfasser: Blomqvist, Jakob, Steuwer, Axel, Bjerkén, Christina, Zanellato, Olivier, Blackmur, Matthew S, Andrieux, Jérôme, Ribeiro, Fabienne
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2015
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article Research Support, Non-U.S. Gov't hydrogen-induced degradation in situ hydrogen charging phase transformation synchrotron X-ray diffraction zirconium hydride
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520 |a For the first time, various hydride phases in a zirconium-hydrogen system have been prepared in a high-energy synchrotron X-ray radiation beamline and their transformation behaviour has been studied in situ. First, the formation and dissolution of hydrides in commercially pure zirconium powder were monitored in real time during hydrogenation and dehydrogenation, then whole pattern crystal structure analysis such as Rietveld and Pawley refinements were performed. All commonly reported low-pressure phases presented in the Zr-H phase diagram are obtained from a single experimental arrangement 
650 4 |a Journal Article 
650 4 |a Research Support, Non-U.S. Gov't 
650 4 |a hydrogen-induced degradation 
650 4 |a in situ hydrogen charging 
650 4 |a phase transformation 
650 4 |a synchrotron X-ray diffraction 
650 4 |a zirconium hydride 
700 1 |a Blomqvist, Jakob  |e verfasserin  |4 aut 
700 1 |a Steuwer, Axel  |e verfasserin  |4 aut 
700 1 |a Bjerkén, Christina  |e verfasserin  |4 aut 
700 1 |a Zanellato, Olivier  |e verfasserin  |4 aut 
700 1 |a Blackmur, Matthew S  |e verfasserin  |4 aut 
700 1 |a Andrieux, Jérôme  |e verfasserin  |4 aut 
700 1 |a Ribeiro, Fabienne  |e verfasserin  |4 aut 
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