Differentiation of enantiomers by 2D NMR spectroscopy at 1 T using residual dipolar couplings

Differentiation of enantiomers by 2D NMR spectroscopy at 1 T using residual dipolar couplings

Copyright © 2015 John Wiley & Sons, Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 54(2016), 6 vom: 14. Juni, Seite 527-30
1. Verfasser: Koos, Martin R M (VerfasserIn)
Weitere Verfasser: Danieli, Ernesto, Casanova, Federico, Blümich, Bernhard, Luy, Burkhard
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2016
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article RDC chiral alignment media differentiation of enantiomers enantiomeric excess low-field NMR
Beschreibung
Zusammenfassung:Copyright © 2015 John Wiley & Sons, Ltd.
Differentiating enantiomers using 2D bench-top NMR spectroscopy. Spectrometers working with permanent magnets at 1 T field strength allow the acquisition of 2D data sets. In conjunction with previously reported chiral alignment media, this setup allows the measurement of enantiomeric excess via residual dipolar couplings in stretched gelatine as a result of the reduced line width obtained by 2D J-resolved spectroscopy
Beschreibung:Date Completed 24.01.2018
Date Revised 24.01.2018
published: Print-Electronic
Citation Status PubMed-not-MEDLINE
ISSN:1097-458X
DOI:10.1002/mrc.4222