Structural evolution of colloidal crystal films in the process of melting revealed by Bragg peak analysis

In situ X-ray diffraction studies of structural evolution of colloidal crystal films formed by polystyrene spherical particles upon incremental heating are reported. The Bragg peak parameters, such as peak position, integrated intensity, and radial and azimuthal widths were analyzed as a function of...

Ausführliche Beschreibung

Bibliographische Detailangaben
Veröffentlicht in:Langmuir : the ACS journal of surfaces and colloids. - 1985. - 31(2015), 19 vom: 19. Mai, Seite 5274-83
1. Verfasser: Sulyanova, Elena A (VerfasserIn)
Weitere Verfasser: Shabalin, Anatoly, Zozulya, Alexey V, Meijer, Janne-Mieke, Dzhigaev, Dmitry, Gorobtsov, Oleg, Kurta, Ruslan P, Lazarev, Sergey, Lorenz, Ulf, Singer, Andrej, Yefanov, Oleksandr, Zaluzhnyy, Ivan, Besedin, Ilya, Sprung, Michael, Petukhov, Andrei V, Vartanyants, Ivan A
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2015
Zugriff auf das übergeordnete Werk:Langmuir : the ACS journal of surfaces and colloids
Schlagworte:Journal Article
LEADER 01000caa a22002652c 4500
001 NLM245398422
003 DE-627
005 20250218013444.0
007 cr uuu---uuuuu
008 231224s2015 xx |||||o 00| ||eng c
024 7 |a 10.1021/la504652z  |2 doi 
028 5 2 |a pubmed25n0817.xml 
035 |a (DE-627)NLM245398422 
035 |a (NLM)25594683 
040 |a DE-627  |b ger  |c DE-627  |e rakwb 
041 |a eng 
100 1 |a Sulyanova, Elena A  |e verfasserin  |4 aut 
245 1 0 |a Structural evolution of colloidal crystal films in the process of melting revealed by Bragg peak analysis 
264 1 |c 2015 
336 |a Text  |b txt  |2 rdacontent 
337 |a ƒaComputermedien  |b c  |2 rdamedia 
338 |a ƒa Online-Ressource  |b cr  |2 rdacarrier 
500 |a Date Completed 16.07.2015 
500 |a Date Revised 19.05.2015 
500 |a published: Print-Electronic 
500 |a Citation Status PubMed-not-MEDLINE 
520 |a In situ X-ray diffraction studies of structural evolution of colloidal crystal films formed by polystyrene spherical particles upon incremental heating are reported. The Bragg peak parameters, such as peak position, integrated intensity, and radial and azimuthal widths were analyzed as a function of temperature. A quantitative study of colloidal crystal lattice distortions and mosaic spread as a function of temperature was carried out using Williamson-Hall plots based on mosaic block model. The temperature dependence of the diameter of polystyrene particles was obtained from the analysis of Bragg peaks, and the form factor contribution extracted from the diffraction patterns. Four stages of structural evolution in a colloidal crystal upon heating were identified. Based on this analysis, a model of the heating and melting process in the colloidal crystal film is suggested 
650 4 |a Journal Article 
700 1 |a Shabalin, Anatoly  |e verfasserin  |4 aut 
700 1 |a Zozulya, Alexey V  |e verfasserin  |4 aut 
700 1 |a Meijer, Janne-Mieke  |e verfasserin  |4 aut 
700 1 |a Dzhigaev, Dmitry  |e verfasserin  |4 aut 
700 1 |a Gorobtsov, Oleg  |e verfasserin  |4 aut 
700 1 |a Kurta, Ruslan P  |e verfasserin  |4 aut 
700 1 |a Lazarev, Sergey  |e verfasserin  |4 aut 
700 1 |a Lorenz, Ulf  |e verfasserin  |4 aut 
700 1 |a Singer, Andrej  |e verfasserin  |4 aut 
700 1 |a Yefanov, Oleksandr  |e verfasserin  |4 aut 
700 1 |a Zaluzhnyy, Ivan  |e verfasserin  |4 aut 
700 1 |a Besedin, Ilya  |e verfasserin  |4 aut 
700 1 |a Sprung, Michael  |e verfasserin  |4 aut 
700 1 |a Petukhov, Andrei V  |e verfasserin  |4 aut 
700 1 |a Vartanyants, Ivan A  |e verfasserin  |4 aut 
773 0 8 |i Enthalten in  |t Langmuir : the ACS journal of surfaces and colloids  |d 1985  |g 31(2015), 19 vom: 19. Mai, Seite 5274-83  |w (DE-627)NLM098181009  |x 1520-5827  |7 nnas 
773 1 8 |g volume:31  |g year:2015  |g number:19  |g day:19  |g month:05  |g pages:5274-83 
856 4 0 |u http://dx.doi.org/10.1021/la504652z  |3 Volltext 
912 |a GBV_USEFLAG_A 
912 |a SYSFLAG_A 
912 |a GBV_NLM 
912 |a GBV_ILN_22 
912 |a GBV_ILN_350 
912 |a GBV_ILN_721 
951 |a AR 
952 |d 31  |j 2015  |e 19  |b 19  |c 05  |h 5274-83