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231224s2014 xx |||||o 00| ||eng c |
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|a 10.1002/adma.201302562
|2 doi
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|a pubmed25n0777.xml
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|a eng
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|a Gu, Xiaodan
|e verfasserin
|4 aut
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|a An in situ grazing incidence X-ray scattering study of block copolymer thin films during solvent vapor annealing
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|c 2014
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|a ƒa Online-Ressource
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|a Date Completed 12.08.2014
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|a Date Revised 30.09.2020
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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|a In situ grazing-incidence small-angle X-ray scattering experiments on thin films of block copolymers during annealing in neutral solvent vapors are reported. By removing the solvent in a controlled manner, the period of the microphase separated morphology is found to increase with increasing block copolymer concentration in a power law manner with an exponent ∼ 2/3. By venting the systems at different rates during the solvent removal process, kinetically arresting the system, the period of the microphase separated morphology in the dried film can be varied
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|a Journal Article
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|a Research Support, Non-U.S. Gov't
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|a Research Support, U.S. Gov't, Non-P.H.S.
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|a block copolymers thin film
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|a in situ GISAXS
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|a lateral ordering and solvent removal rates
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|a solvent vapor annealing
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|a Gunkel, Ilja
|e verfasserin
|4 aut
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|a Hexemer, Alexander
|e verfasserin
|4 aut
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|a Gu, Weiyin
|e verfasserin
|4 aut
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|a Russell, Thomas P
|e verfasserin
|4 aut
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|t Advanced materials (Deerfield Beach, Fla.)
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|g 26(2014), 2 vom: 15. Jan., Seite 273-81
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|g volume:26
|g year:2014
|g number:2
|g day:15
|g month:01
|g pages:273-81
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|u http://dx.doi.org/10.1002/adma.201302562
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