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231224s2012 xx |||||o 00| ||eng c |
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|a 10.1107/S0909049512023801
|2 doi
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|a eng
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|a Chen, Gang
|e verfasserin
|4 aut
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|a Structure determination of Pt-coated Au dumbbells via fluctuation X-ray scattering
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|c 2012
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
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|2 rdamedia
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|a ƒa Online-Ressource
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|a Date Completed 10.01.2013
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|a Date Revised 17.08.2012
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a A fluctuation X-ray scattering experiment has been carried out on platinum-coated gold nanoparticles randomly oriented on a substrate. A complete algorithm for determining the electron density of an individual particle from diffraction patterns of many particles randomly oriented about a single axis is demonstrated. This algorithm operates on angular correlations among the measured intensity distributions and recovers the angular correlation functions of a single particle from measured diffraction patterns. Taking advantage of the cylindrical symmetry of the nanoparticles, a cylindrical slice model is proposed to reconstruct the structure of the nanoparticles by fitting the experimental ring angular auto-correlation and small-angle scattering data obtained from many scattering patterns. The physical meaning of the refined structure is discussed in terms of their statistical distributions of the shape and electron density profile
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|a Journal Article
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|a Research Support, U.S. Gov't, Non-P.H.S.
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|a Modestino, Miguel A
|e verfasserin
|4 aut
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|a Poon, Billy K
|e verfasserin
|4 aut
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|a Schirotzek, André
|e verfasserin
|4 aut
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|a Marchesini, Stefano
|e verfasserin
|4 aut
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|a Segalman, Rachel A
|e verfasserin
|4 aut
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|a Hexemer, Alexander
|e verfasserin
|4 aut
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|a Zwart, Peter H
|e verfasserin
|4 aut
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|i Enthalten in
|t Journal of synchrotron radiation
|d 1994
|g 19(2012), Pt 5 vom: 05. Sept., Seite 695-700
|w (DE-627)NLM09824129X
|x 1600-5775
|7 nnns
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|g volume:19
|g year:2012
|g number:Pt 5
|g day:05
|g month:09
|g pages:695-700
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|u http://dx.doi.org/10.1107/S0909049512023801
|3 Volltext
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