Aligned deuterochloroform in cross-linked polystyrene as a new sample for adjusting the magic angle in HR-MAS
Copyright © 2012 John Wiley & Sons, Ltd.
| Publié dans: | Magnetic resonance in chemistry : MRC. - 1985. - 50(2012), 1 vom: 27. Jan., Seite 5-6 |
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| Auteur principal: | |
| Autres auteurs: | , |
| Format: | Article en ligne |
| Langue: | English |
| Publié: |
2012
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| Accès à la collection: | Magnetic resonance in chemistry : MRC |
| Sujets: | Journal Article Polystyrenes Chloroform 7V31YC746X Deuterium AR09D82C7G |
| Résumé: | Copyright © 2012 John Wiley & Sons, Ltd. A new and easily usable sample for adjusting the magic angle in a high resolution magic angle spinning (HR-MAS) probe head is a swollen polymer stick in CDCl(3) . The deuterium resonance shows a quadrupolar splitting if the rotor assembly is not at the magic angle, but a sharp singlet if the magic angle is correctly adjusted |
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| Description: | Date Completed 23.08.2012 Date Revised 21.11.2013 published: Print-Electronic Citation Status MEDLINE |
| ISSN: | 1097-458X |
| DOI: | 10.1002/mrc.3789 |