Fast X-ray microdiffraction techniques for studying irreversible transformations in materials

A pair of techniques have been developed for performing time-resolved X-ray microdiffraction on irreversible phase transformations. In one technique capillary optics are used to focus a high-flux broad-spectrum X-ray beam to a 60 µm spot size and a fast pixel array detector is used to achieve tempor...

Ausführliche Beschreibung

Bibliographische Detailangaben
Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 18(2011), Pt 3 vom: 18. Mai, Seite 464-74
1. Verfasser: Kelly, Stephen T (VerfasserIn)
Weitere Verfasser: Trenkle, Jonathan C, Koerner, Lucas J, Barron, Sara C, Walker, Nöel, Pouliquen, Philippe O, Tate, Mark W, Gruner, Sol M, Dufresne, Eric M, Weihs, Timothy P, Hufnagel, Todd C
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2011
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article
LEADER 01000naa a22002652 4500
001 NLM207785074
003 DE-627
005 20231224002826.0
007 cr uuu---uuuuu
008 231224s2011 xx |||||o 00| ||eng c
024 7 |a 10.1107/S0909049511002640  |2 doi 
028 5 2 |a pubmed24n0693.xml 
035 |a (DE-627)NLM207785074 
035 |a (NLM)21525656 
040 |a DE-627  |b ger  |c DE-627  |e rakwb 
041 |a eng 
100 1 |a Kelly, Stephen T  |e verfasserin  |4 aut 
245 1 0 |a Fast X-ray microdiffraction techniques for studying irreversible transformations in materials 
264 1 |c 2011 
336 |a Text  |b txt  |2 rdacontent 
337 |a ƒaComputermedien  |b c  |2 rdamedia 
338 |a ƒa Online-Ressource  |b cr  |2 rdacarrier 
500 |a Date Completed 16.08.2011 
500 |a Date Revised 20.10.2021 
500 |a published: Print-Electronic 
500 |a Citation Status PubMed-not-MEDLINE 
520 |a A pair of techniques have been developed for performing time-resolved X-ray microdiffraction on irreversible phase transformations. In one technique capillary optics are used to focus a high-flux broad-spectrum X-ray beam to a 60 µm spot size and a fast pixel array detector is used to achieve temporal resolution of 55 µs. In the second technique the X-rays are focused with Kirkpatrick-Baez mirrors to achieve a spatial resolution better than 10 µm and a fast shutter is used to provide temporal resolution better than 20 µs while recording the diffraction pattern on a (relatively slow) X-ray CCD camera. Example data from experiments are presented where these techniques are used to study self-propagating high-temperature synthesis reactions in metal laminate foils 
650 4 |a Journal Article 
700 1 |a Trenkle, Jonathan C  |e verfasserin  |4 aut 
700 1 |a Koerner, Lucas J  |e verfasserin  |4 aut 
700 1 |a Barron, Sara C  |e verfasserin  |4 aut 
700 1 |a Walker, Nöel  |e verfasserin  |4 aut 
700 1 |a Pouliquen, Philippe O  |e verfasserin  |4 aut 
700 1 |a Tate, Mark W  |e verfasserin  |4 aut 
700 1 |a Gruner, Sol M  |e verfasserin  |4 aut 
700 1 |a Dufresne, Eric M  |e verfasserin  |4 aut 
700 1 |a Weihs, Timothy P  |e verfasserin  |4 aut 
700 1 |a Hufnagel, Todd C  |e verfasserin  |4 aut 
773 0 8 |i Enthalten in  |t Journal of synchrotron radiation  |d 1994  |g 18(2011), Pt 3 vom: 18. Mai, Seite 464-74  |w (DE-627)NLM09824129X  |x 1600-5775  |7 nnns 
773 1 8 |g volume:18  |g year:2011  |g number:Pt 3  |g day:18  |g month:05  |g pages:464-74 
856 4 0 |u http://dx.doi.org/10.1107/S0909049511002640  |3 Volltext 
912 |a GBV_USEFLAG_A 
912 |a SYSFLAG_A 
912 |a GBV_NLM 
912 |a GBV_ILN_40 
912 |a GBV_ILN_350 
912 |a GBV_ILN_2005 
951 |a AR 
952 |d 18  |j 2011  |e Pt 3  |b 18  |c 05  |h 464-74