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|a pubmed24n0616.xml
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|a (DE-627)NLM184638488
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|a (NLM)19024725
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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|a Ince, Muharrem
|e verfasserin
|4 aut
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|a Solid-phase extraction and preconcentration of copper in mineral waters with 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 and flame atomic absorption spectrometry
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|c 2008
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Completed 20.03.2009
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|a Date Revised 23.09.2019
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|a published: Print
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|a Citation Status MEDLINE
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|a A simple, sensitive, accurate, and selective method for determination of ultratrace levels of copper is modified. The method is based on preconcentration of copper on the 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 (non-ionic copoly[styrene-acrylic compound]) at pH 5.0 to 6.5 for contact time as low as 45 minutes. The adsorbed copper was eluted with concentrated nitric acid and measured by flame atomic absorption spectrometry. Recoveries of up to 90% were achieved. The optimized preconcentration method was applied to copper determination in various water samples. The detection limit was found to be 0.09 ng mL(-1). The relative standard deviation was found to be 9% using 300 mL of 5.0 ng mL(-1) for 10 replicate preconcentration procedures. Copper concentrations in the studied water samples were found to be in the ranges of 0.4 to 18.0 ng mL(-1)
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|a Journal Article
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|a Acrylic Resins
|2 NLM
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|a Mineral Waters
|2 NLM
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|a Polystyrenes
|2 NLM
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|a Resorcinols
|2 NLM
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|a Water Pollutants, Chemical
|2 NLM
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|a amberlite XAD 7
|2 NLM
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|a 37380-43-1
|2 NLM
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|a Copper
|2 NLM
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|a 789U1901C5
|2 NLM
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|a 4-(2-pyridylazo)resorcinol
|2 NLM
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|a N68T40H95T
|2 NLM
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|a Kaplan, Olcay
|e verfasserin
|4 aut
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|a Yaman, Mehmet
|e verfasserin
|4 aut
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|i Enthalten in
|t Water environment research : a research publication of the Water Environment Federation
|d 1998
|g 80(2008), 11 vom: 15. Nov., Seite 2104-10
|w (DE-627)NLM098214292
|x 1554-7531
|7 nnns
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|g volume:80
|g year:2008
|g number:11
|g day:15
|g month:11
|g pages:2104-10
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|a GBV_USEFLAG_A
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|a SYSFLAG_A
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|a GBV_NLM
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|a GBV_ILN_350
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|a AR
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|d 80
|j 2008
|e 11
|b 15
|c 11
|h 2104-10
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