Solid-phase extraction and preconcentration of copper in mineral waters with 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 and flame atomic absorption spectrometry

A simple, sensitive, accurate, and selective method for determination of ultratrace levels of copper is modified. The method is based on preconcentration of copper on the 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 (non-ionic copoly[styrene-acrylic compound]) at pH 5.0 to 6.5 for contact tim...

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Veröffentlicht in:Water environment research : a research publication of the Water Environment Federation. - 1998. - 80(2008), 11 vom: 15. Nov., Seite 2104-10
1. Verfasser: Ince, Muharrem (VerfasserIn)
Weitere Verfasser: Kaplan, Olcay, Yaman, Mehmet
Format: Aufsatz
Sprache:English
Veröffentlicht: 2008
Zugriff auf das übergeordnete Werk:Water environment research : a research publication of the Water Environment Federation
Schlagworte:Journal Article Acrylic Resins Mineral Waters Polystyrenes Resorcinols Water Pollutants, Chemical amberlite XAD 7 37380-43-1 Copper 789U1901C5 mehr... 4-(2-pyridylazo)resorcinol N68T40H95T
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100 1 |a Ince, Muharrem  |e verfasserin  |4 aut 
245 1 0 |a Solid-phase extraction and preconcentration of copper in mineral waters with 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 and flame atomic absorption spectrometry 
264 1 |c 2008 
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500 |a Date Completed 20.03.2009 
500 |a Date Revised 23.09.2019 
500 |a published: Print 
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520 |a A simple, sensitive, accurate, and selective method for determination of ultratrace levels of copper is modified. The method is based on preconcentration of copper on the 4-(2-pyridyl-azo) resorcinol-loaded amberlite XAD-7 (non-ionic copoly[styrene-acrylic compound]) at pH 5.0 to 6.5 for contact time as low as 45 minutes. The adsorbed copper was eluted with concentrated nitric acid and measured by flame atomic absorption spectrometry. Recoveries of up to 90% were achieved. The optimized preconcentration method was applied to copper determination in various water samples. The detection limit was found to be 0.09 ng mL(-1). The relative standard deviation was found to be 9% using 300 mL of 5.0 ng mL(-1) for 10 replicate preconcentration procedures. Copper concentrations in the studied water samples were found to be in the ranges of 0.4 to 18.0 ng mL(-1) 
650 4 |a Journal Article 
650 7 |a Acrylic Resins  |2 NLM 
650 7 |a Mineral Waters  |2 NLM 
650 7 |a Polystyrenes  |2 NLM 
650 7 |a Resorcinols  |2 NLM 
650 7 |a Water Pollutants, Chemical  |2 NLM 
650 7 |a amberlite XAD 7  |2 NLM 
650 7 |a 37380-43-1  |2 NLM 
650 7 |a Copper  |2 NLM 
650 7 |a 789U1901C5  |2 NLM 
650 7 |a 4-(2-pyridylazo)resorcinol  |2 NLM 
650 7 |a N68T40H95T  |2 NLM 
700 1 |a Kaplan, Olcay  |e verfasserin  |4 aut 
700 1 |a Yaman, Mehmet  |e verfasserin  |4 aut 
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