Structure elucidation and NMR assignments for two amide alkaloids from a Mangrove endophytic Fungus (No. ZZF-22)

2008 John Wiley & Sons, Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 47(2009), 1 vom: 30. Jan., Seite 92-5
1. Verfasser: Chen, Yiguang (VerfasserIn)
Weitere Verfasser: Shao, Changlun, Huang, Zhongjing, Zhang, Ying, Cai, Xiaoling, She, Zhigang, Zhou, Shining, Lin, Yongcheng
Format: Online-Aufsatz
Sprache:English
Veröffentlicht: 2009
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article Research Support, Non-U.S. Gov't Alkaloids Amides Biological Products Carbon Isotopes
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520 |a The structure elucidations and complete (1)H and (13)C NMR assignments are reported for two new natural products: 3-benzylidene-8,8a-dihydroxy-2-methyl-hexahydro-pyrrolo[1,2-a]pyrazine-1,4-dione(1) and 4-hydroxy-6-(hydroxy-phenyl-methyl)-N-(3-methyl-butyryl)-nicotinamide (2). Both of these secondary metabolites were isolated from the fermentation medium of a Mangrove endophytic fungus. High resolution electron impact mass spectrometry (HREIMS), FT-IR Spectroscopy and NMR experiments including gCOSY, gHMQC, gHMBC and NOE were used for determination of the structures and assignments of the amide alkaloids 
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700 1 |a She, Zhigang  |e verfasserin  |4 aut 
700 1 |a Zhou, Shining  |e verfasserin  |4 aut 
700 1 |a Lin, Yongcheng  |e verfasserin  |4 aut 
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