Application of a pnCCD in X-ray diffraction : a three-dimensional X-ray detector
The first application of a pnCCD detector for X-ray scattering experiments using white synchrotron radiation at BESSY II is presented. A Cd arachidate multilayer was investigated in reflection geometry within the energy range 7 keV < E < 35 keV. At fixed angle of incidence the two-dimensional...
Veröffentlicht in: | Journal of synchrotron radiation. - 1994. - 15(2008), Pt 5 vom: 21. Sept., Seite 449-57 |
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1. Verfasser: | |
Weitere Verfasser: | , , , , |
Format: | Online-Aufsatz |
Sprache: | English |
Veröffentlicht: |
2008
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Zugriff auf das übergeordnete Werk: | Journal of synchrotron radiation |
Schlagworte: | Journal Article Research Support, Non-U.S. Gov't |
Zusammenfassung: | The first application of a pnCCD detector for X-ray scattering experiments using white synchrotron radiation at BESSY II is presented. A Cd arachidate multilayer was investigated in reflection geometry within the energy range 7 keV < E < 35 keV. At fixed angle of incidence the two-dimensional diffraction pattern containing several multilayer Bragg peaks and respective diffuse-resonant Bragg sheets were observed. Since every pixel of the detector is able to determine the energy of every incoming photon with a resolution DeltaE/E approximately 10(-2), a three-dimensional dataset is finally obtained. In order to achieve this energy resolution the detector was operated in the so-called single-photon-counting mode. A full dataset was evaluated taking into account all photons recorded within 10(5) detector frames at a readout rate of 200 Hz. By representing the data in reciprocal-space coordinates, it becomes obvious that this experiment with the pnCCD detector provides the same information as that obtained by combining a large number of monochromatic scattering experiments using conventional area detectors |
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Beschreibung: | Date Completed 09.10.2008 Date Revised 27.08.2008 published: Print-Electronic Citation Status MEDLINE |
ISSN: | 1600-5775 |
DOI: | 10.1107/S0909049508018931 |