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231223s2008 xx |||||o 00| ||eng c |
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|a 10.1021/la801343b
|2 doi
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|a pubmed24n0603.xml
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|a eng
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| 100 |
1 |
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|a Crowe, Loretta L
|e verfasserin
|4 aut
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| 245 |
1 |
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|a Silica passivation efficiency monitored by a surface-bound fluorescent dye
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|c 2008
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|a Text
|b txt
|2 rdacontent
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|a ƒaComputermedien
|b c
|2 rdamedia
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|a ƒa Online-Ressource
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|2 rdacarrier
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|a Date Completed 17.09.2008
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|a Date Revised 13.08.2008
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|a published: Print-Electronic
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|a Citation Status PubMed-not-MEDLINE
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|a A new method for evaluating surface passivation of silicon surfaces using a strongly adsorbing and fluorescing perylenediimide (PDI) dye is reported. Silanes containing differing reactive groups delivering a trimethylsilyl moiety were investigated for their ability to passivate glass surfaces, both from solution and in the vapor phase, as a function of temperature and concentration. Among the silanizing agents used in this study were 1,1,1,3,3,3-hexamethyldisilazane ( HMDS), allyltrimethylsilane ( TMS-A), chlorotrimethylsilane ( TMS-Cl), N-(trimethylsilyl)imidazole ( TMS-Im), and N, N-dimethylaminotrimethylsilane ( TMS-DMA). Surface coverage was determined using fluorescence intensity. The highest surface coverage films were obtained on glass treated with HMDS vapor at 280 degrees C or with solutions of TMS-Im or TMS-DMA at 105 degrees C. These studies provide important insight into the optimal methods for surface passivation
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|a Journal Article
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1 |
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|a Tolbert, Laren M
|e verfasserin
|4 aut
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| 773 |
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|i Enthalten in
|t Langmuir : the ACS journal of surfaces and colloids
|d 1992
|g 24(2008), 16 vom: 19. Aug., Seite 8541-6
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|g volume:24
|g year:2008
|g number:16
|g day:19
|g month:08
|g pages:8541-6
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|u http://dx.doi.org/10.1021/la801343b
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