Complete assignments of (1)H and (13)C NMR spectral data of nine surfactin isomers
A new surfactin isomer (1) was isolated from a mangrove bacteria strain 'Bacillus sp'. Its structure was identified, and full assignments of (1)H and (13)C NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments including DEPT,...
| Veröffentlicht in: | Magnetic resonance in chemistry : MRC. - 1985. - 45(2007), 9 vom: 03. Sept., Seite 792-6 |
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| 1. Verfasser: | |
| Weitere Verfasser: | , , , , , , |
| Format: | Aufsatz |
| Sprache: | English |
| Veröffentlicht: |
2007
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| Zugriff auf das übergeordnete Werk: | Magnetic resonance in chemistry : MRC |
| Schlagworte: | Journal Article Research Support, Non-U.S. Gov't Amino Acids Fatty Acids Indicators and Reagents Peptides, Cyclic Solvents Bromcresol Green 8YGN0Y942M Dimethyl Sulfoxide |
| Zusammenfassung: | A new surfactin isomer (1) was isolated from a mangrove bacteria strain 'Bacillus sp'. Its structure was identified, and full assignments of (1)H and (13)C NMR spectral data were achieved for the first time by a combination of mass spectrometry and 1D and 2D NMR experiments including DEPT, (1)H-(1)H COSY, HSQC, HMBC, TOCSY, ROESY, and HSQC-TOCSY. The NMR spectral data of eight known analogs (2-9) are also reported |
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| Beschreibung: | Date Completed 12.10.2007 Date Revised 21.11.2013 published: Print Citation Status MEDLINE |
| ISSN: | 1097-458X |