Structure elucidation and complete NMR spectral assignments of three new lanostanoid triterpenes with unprecedented Delta(16, 17) double bond from Ganoderma lucidum

Three new lanostanoid triterpenes named 3beta,7beta-di- hydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid (1), 3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester (2), and 12beta-acetoxy-3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid (3) were isolat...

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Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 45(2007), 9 vom: 03. Sept., Seite 789-91
1. Verfasser: Guan, Shu-Hong (VerfasserIn)
Weitere Verfasser: Yang, Min, Wang, Xiao-Ming, Xia, Jia-Meng, Zhang, Zhi-Ming, Liu, Xuan, Guo, De-An
Format: Aufsatz
Sprache:English
Veröffentlicht: 2007
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article 12beta-acetoxy-3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid 3beta,7beta-di- hydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid 3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester Triterpenes Lanosterol 1J05Z83K3M
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245 1 0 |a Structure elucidation and complete NMR spectral assignments of three new lanostanoid triterpenes with unprecedented Delta(16, 17) double bond from Ganoderma lucidum 
264 1 |c 2007 
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500 |a Date Completed 12.10.2007 
500 |a Date Revised 21.11.2013 
500 |a published: Print 
500 |a Citation Status MEDLINE 
520 |a Three new lanostanoid triterpenes named 3beta,7beta-di- hydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid (1), 3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid methyl ester (2), and 12beta-acetoxy-3beta,7beta-dihydroxy-11,15,23-trioxo-lanost-8,16-dien-26-oic acid (3) were isolated from the fruit bodies of Ganoderma lucidum. They all show a Delta(16, 17) double bond unprecedented in such types of lanostanoid triterpenes possessing the side chain at C-17. The complete NMR assignments for these compounds were carried out using (1)H, (13)C, DEPT, COSY, HSQC, HMBC, and ROESY NMR experiments 
650 4 |a Journal Article 
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700 1 |a Yang, Min  |e verfasserin  |4 aut 
700 1 |a Wang, Xiao-Ming  |e verfasserin  |4 aut 
700 1 |a Xia, Jia-Meng  |e verfasserin  |4 aut 
700 1 |a Zhang, Zhi-Ming  |e verfasserin  |4 aut 
700 1 |a Liu, Xuan  |e verfasserin  |4 aut 
700 1 |a Guo, De-An  |e verfasserin  |4 aut 
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