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|a (NLM)17559164
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|a DE-627
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|e rakwb
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|a eng
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|a Lakshmi Devi, A Siva
|e verfasserin
|4 aut
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|a Structure elucidation of thermal degradation products of amlodipine
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|c 2007
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Completed 24.10.2007
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|a Date Revised 21.11.2013
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|a published: Print
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|a Citation Status MEDLINE
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|a Copyright 2007 John Wiley & Sons, Ltd.
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|a Thermal degradation of amlodipine base causes intramolecular reactions affording three cyclic products, referred to as AMLDEG-I, AMLDEG-II, and AMLDEG-III, respectively. AMLDEG-I is a cyclized product formed by intramolecular elimination of ammonia from amlodipine. AMLDEG-II is a positional isomer of AMLDEG-I. AMLDEG-III is also intramolecular cyclisation product. The three degradation products were isolated by column chromatography and characterized by FT-IR and 1H and 13C NMR spectroscopy data. The AMLDEG-III was crystallized and its structure was solved by single crystal X-ray diffraction (SXRD)
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|a Journal Article
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|a Amlodipine
|2 NLM
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|a 1J444QC288
|2 NLM
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|a Srinivasa Rao, Y
|e verfasserin
|4 aut
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|a Satish, M
|e verfasserin
|4 aut
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|a Jyothi, G
|e verfasserin
|4 aut
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|a Babu Rao, K
|e verfasserin
|4 aut
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|a Omdutt, T
|e verfasserin
|4 aut
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 45(2007), 8 vom: 01. Aug., Seite 688-91
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnas
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|g volume:45
|g year:2007
|g number:8
|g day:01
|g month:08
|g pages:688-91
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|d 45
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