Two-dimensional spectroscopy with parallel acquisition of 1H-X and 19F-X correlations

Copyright (c) 2007 John Wiley & Sons, Ltd.

Bibliographische Detailangaben
Veröffentlicht in:Magnetic resonance in chemistry : MRC. - 1985. - 45(2007), 5 vom: 15. Mai, Seite 378-80
1. Verfasser: Kupce, Eriks (VerfasserIn)
Weitere Verfasser: Cheatham, Steve, Freeman, Ray
Format: Aufsatz
Sprache:English
Veröffentlicht: 2007
Zugriff auf das übergeordnete Werk:Magnetic resonance in chemistry : MRC
Schlagworte:Journal Article 2-bromophenyl-3-trifluoromethyl-5-methylpyrazole Carbon Isotopes Nitrogen Isotopes Protons Pyrazoles Fluorine 284SYP0193
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520 |a Two-dimensional NMR spectra correlating both (1)H and (19)F nuclei with either (13)C or (15)N, are recorded at the same time, using a 600-MHz broadband radio frequency probe feeding independent (1)H and (19)F receiver channels. This technique, known as parallel acquisition NMR spectroscopy (PANSY), speeds up multidimensional NMR and is compatible with other fast-acquisition schemes. The method is illustrated with single-bond (HSQC) and multiple-bond (HMBC) experiments on 2-bromophenyl-3-trifluoromethyl-5-methylpyrazole, giving simultaneous (1)H-X and (19)F-X correlation spectra (X = (13) C or (15)N) 
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