Three-dimensional visualization of the inner structure of single crystals by step-scanning white X-ray section topography

Visualization of the three-dimensional distribution of the crystal defects of large single crystals of calcium fluoride has been demonstrated by white X-ray section topography using sheet-like X-rays (BL28B2 at SPring-8). An image of the three-dimensional distribution of the crystal defects was reco...

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Veröffentlicht in:Journal of synchrotron radiation. - 1994. - 13(2006), Pt 6 vom: 15. Nov., Seite 484-8
1. Verfasser: Mukaide, Taihei (VerfasserIn)
Weitere Verfasser: Kajiwara, Kentaro, Noma, Takashi, Takada, Kazuhiro
Format: Aufsatz
Sprache:English
Veröffentlicht: 2006
Zugriff auf das übergeordnete Werk:Journal of synchrotron radiation
Schlagworte:Journal Article Calcium Fluoride O3B55K4YKI
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245 1 0 |a Three-dimensional visualization of the inner structure of single crystals by step-scanning white X-ray section topography 
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520 |a Visualization of the three-dimensional distribution of the crystal defects of large single crystals of calcium fluoride has been demonstrated by white X-ray section topography using sheet-like X-rays (BL28B2 at SPring-8). An image of the three-dimensional distribution of the crystal defects was reconstructed by stacking section topographs, which expressed the images of cross sections of the sample. The section topographs were recorded using a CMOS flat-panel imager or a CCD detector combined with scintillator (Gd(2)O(2)S:Tb) and relay lens system. The section topographs were measured by repeating cycles of exposure and sample translation along the direction perpendicular to the top face of the sample. Using high-brilliance and high-energy white X-rays ( approximately 60 keV) efficiently, visualization of the three-dimensional structure of subgrains of a sample of up to 60 mm in diameter was achieved. Furthermore, the three-dimensional distribution of the glide plane in the crystal was visualized by reconstructing the linear contrast of the glide plane 
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700 1 |a Kajiwara, Kentaro  |e verfasserin  |4 aut 
700 1 |a Noma, Takashi  |e verfasserin  |4 aut 
700 1 |a Takada, Kazuhiro  |e verfasserin  |4 aut 
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