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231223s2006 xx ||||| 00| ||eng c |
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|a eng
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| 100 |
1 |
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|a Mizuno, Mikihisa
|e verfasserin
|4 aut
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| 245 |
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|a High-yield sol-gel synthesis of well-dispersed, colorless ZrO(2) nanocrystals
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|c 2006
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|a Text
|b txt
|2 rdacontent
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| 337 |
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Completed 17.08.2007
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|a Date Revised 08.08.2006
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|a published: Print
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|a Citation Status PubMed-not-MEDLINE
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|a A 93% high-yield synthesis of well-dispersed, colorless zirconium dioxide (ZrO(2)) nanocrystals is reported. In this synthesis, hydrolysis and condensation reactions of zirconium(IV) tert-butoxide in the presence of oleic acid (100 degrees C) formed ZrO(2) precursors. The ZrO(2) precursors were made of -Zr-O-Zr- networks surrounded by oleic acid molecules. Annealing (280 degrees C) the precursors dispersed in dioctyl ether caused crystallization of the -Zr-O-Zr- networks, thereby generating 4 nm ZrO(2) nanocrystals stabilized with oleic acid. The particles were highly crystalline and tetragonal phase. A dense ZrO(2) nanocrystal dispersion in toluene (280 mg/mL) showed a transmittance of about 90% (3 mm optical path length) in the whole visible region
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|a Journal Article
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|a Sasaki, Yuichi
|e verfasserin
|4 aut
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1 |
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|a Lee, Sungkil
|e verfasserin
|4 aut
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| 700 |
1 |
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|a Katakura, Hitoshi
|e verfasserin
|4 aut
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| 773 |
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8 |
|i Enthalten in
|t Langmuir : the ACS journal of surfaces and colloids
|d 1985
|g 22(2006), 17 vom: 15. Aug., Seite 7137-40
|w (DE-627)NLM098181009
|x 1520-5827
|7 nnas
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| 773 |
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|g volume:22
|g year:2006
|g number:17
|g day:15
|g month:08
|g pages:7137-40
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|d 22
|j 2006
|e 17
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|h 7137-40
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