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|a (DE-627)NLM164085157
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|a (NLM)16835898
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|a DE-627
|b ger
|c DE-627
|e rakwb
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|a eng
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|a Fontana, Gianfranco
|e verfasserin
|4 aut
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|a Complete 1H and 13C NMR assignments of clerodane diterpenoids of Salvia splendens
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|c 2006
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|a Text
|b txt
|2 rdacontent
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|a ohne Hilfsmittel zu benutzen
|b n
|2 rdamedia
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|a Band
|b nc
|2 rdacarrier
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|a Date Completed 05.09.2007
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|a Date Revised 21.11.2013
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|a published: Print
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|a Citation Status MEDLINE
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|a Copyright (c) 2006 John Wiley & Sons, Ltd.
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|a Unambiguous and complete assignments of 1H and 13C NMR chemical shifts for five clerodane diterpenes, four of them isolated from Salvia splendens (salviarin, splendidin and splenolides A and B) and one obtained by acetylation of splenolide A, are presented. The assignments are based on 2D shift-correlated [1H,1H-COSY, 1H,13C-gHSQC-1J(C,H) and 1H,13C-gHMBC-nJ(C,H) (n=2 and 3)] and nuclear Overhauser effect (NOE) experiments. The conformation of the rings of these compounds is supported by the 3J(H,H) values and NOE results
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|a Journal Article
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|a Research Support, Non-U.S. Gov't
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|a Carbon Isotopes
|2 NLM
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|a Diterpenes, Clerodane
|2 NLM
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|a Hydrogen
|2 NLM
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|a 7YNJ3PO35Z
|2 NLM
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|a Savona, Giuseppe
|e verfasserin
|4 aut
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|a Rodríguez, Benjamín
|e verfasserin
|4 aut
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|i Enthalten in
|t Magnetic resonance in chemistry : MRC
|d 1985
|g 44(2006), 10 vom: 01. Okt., Seite 962-5
|w (DE-627)NLM098179667
|x 1097-458X
|7 nnns
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|g volume:44
|g year:2006
|g number:10
|g day:01
|g month:10
|g pages:962-5
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|d 44
|j 2006
|e 10
|b 01
|c 10
|h 962-5
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