Complete 1H and 13C assignments of fluorinated analogs of dehydroepiandrosterone
Copyright 2006 John Wiley & Sons, Ltd.
| Publié dans: | Magnetic resonance in chemistry : MRC. - 1985. - 44(2006), 11 vom: 04. Nov., Seite 1051-3 |
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| Auteur principal: | |
| Autres auteurs: | , , |
| Format: | Article |
| Langue: | English |
| Publié: |
2006
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| Accès à la collection: | Magnetic resonance in chemistry : MRC |
| Sujets: | Journal Article Research Support, N.I.H., Extramural Carbon Isotopes Protons Fluorine 284SYP0193 Dehydroepiandrosterone 459AG36T1B |
| Résumé: | Copyright 2006 John Wiley & Sons, Ltd. The complete assignments of all 1H and 13C chemical shifts were made for the fluorinated dehydroepiandrosterone (DHEA) analog fluasterone, 2, and two potential in vivo metabolites 3 and 4. The assignments were made using a combination of one- and two-dimensional NMR techniques (1H, 13C, gDQCOSY, gHSQC, gHMBC). Once the proton chemical shifts were assigned, the stereochemistry of the two hydroxylated analogs was determined using 2D ROESY experiments |
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| Description: | Date Completed 05.03.2007 Date Revised 21.11.2013 published: Print Citation Status MEDLINE |
| ISSN: | 1097-458X |